2,3-Dimercapto-1-propanol synthesis
- Product Name:2,3-Dimercapto-1-propanol
- CAS Number:59-52-9
- Molecular formula:C3H8OS2
- Molecular Weight:124.22
96-13-9
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59-52-9
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Yield:59-52-9 58%
Reaction Conditions:
Stage #1: with sulfur;ethanolamine;hydrazine in water at 70 - 73; for 2.5 h;
Stage #2:2,3-Dibromopropan-1-ol with ethanolamine;hydrazine in water at 45 - 50; for 2 h;
Stage #3: with potassium hydroxide;hydrazine in water at 80; for 2 h;Inert atmosphere;
References:
Levanova;Grabel'nykh;Sukhomazova;Zemirova;Russavskaya;Albanov;Klyba;Zhanchipova;Korchevin [Russian Journal of Organic Chemistry,2008,vol. 44,# 10,p. 1428 - 1433] Location in patent:experimental part
106-89-8
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27550-66-9
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584-04-3
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59-52-9
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616-23-9
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59-52-9
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![Ethanethioic acid, S,S'-[1-[(acetyloxy)methyl]-1,2-ethanediyl] ester (9CI)](/CAS/20210305/GIF/59051-15-9.gif)
59051-15-9
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59-52-9
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