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ChemicalBook CAS DataBase List 2,3,4,5,6,7-Hexahydro-1H-indene-1-one
22118-00-9

2,3,4,5,6,7-Hexahydro-1H-indene-1-one synthesis

4synthesis methods
-

Yield:-

Steps:

Multi-step reaction with 5 steps
1: 85 percent / CuI; diethylamine / Pd(PPh3)2Cl2 / toluene / 12 h / 28 °C
2: 82 percent / NaBH4 / methanol / 0.5 h / 0 °C
3: 89 percent / imidazole / dimethylformamide / 5 h / 0 °C
4: 93 percent / K2CO3; MeOH / CH2Cl2 / 25 °C
5: 63 percent / TpRuPPh3(MeCN)2SbF6 / toluene / 20 h / 105 °C

References:

Odedra, Arjan;Datta, Swarup;Liu, Rai-Shung [Journal of Organic Chemistry,2007,vol. 72,# 9,p. 3289 - 3292]

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Cyclohexene, 1-bromo-2-ethenyl-

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