2,2',4,4'-TETRABROMODIPHENYL ETHER synthesis

4synthesis methods

Product Name:2,2',4,4'-TETRABROMODIPHENYL ETHER
CAS Number:5436-43-1
Molecular formula:C12H6Br4O
Molecular Weight:485.79

615-58-7
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5436-43-1
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$94.00/100mg

Yield:5436-43-1 89%

Reaction Conditions:

for 0.2 h;Reagent/catalyst;

Steps:

1 Example 1Preparation of tetrabromobiphenyl ether-47
SiO2-Zr2 (0.05g) and 2,4-dibromophenol (2.50g) were mixed in a mortar and ground for 12 minutes,The product was separated by silica gel column chromatography using n-pentane as eluent to give 2.16 g of a white solid in 89% yield.

References:

Shandong Analysis Beta Center;Ji Wenhua;Zhao Rusong;Wang Xiao;Geng Yanling;Wang Xia CN106957218, 2017, A Location in patent:Paragraph 0043-0047

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615-58-7
211 suppliers
$10.00/500mg