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138227-68-6

1N-BOC 4-(2'-METHYL-4'-NITROPHENOXY) PIPERIDINE synthesis

4synthesis methods
109384-19-2 Synthesis
N-BOC-4-Hydroxypiperidine

109384-19-2
470 suppliers
$5.00/1g

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Yield:138227-68-6 107 g

Reaction Conditions:

Stage #1: t-butyl 4-hydroxy piperidine-1-carboxylatewith sodium hydride in N,N-dimethyl-formamide at 10 - 15; for 0.5 h;
Stage #2: 5-nitro-2-fluorotoluene in N,N-dimethyl-formamide at 20; for 3 h;Further stages.;

References:

Lippa, Blaise;Kauffman, Goss S.;Arcari, Joel;Kwan, Tricia;Chen, Jinshan;Hungerford, William;Bhattacharya, Samit;Zhao, Xumiao;Williams, Courtney;Xiao, Jun;Pustilnik, Leslie;Su, Chunyan;Moyer, James D.;Ma, Ling;Campbell, Mary;Steyn, Stefanus [Bioorganic and Medicinal Chemistry Letters,2007,vol. 17,# 11,p. 3081 - 3086]

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