1-METHYL-1,2,4-TRIAZOLE synthesis
- Product Name:1-METHYL-1,2,4-TRIAZOLE
- CAS Number:6086-21-1
- Molecular formula:C3H5N3
- Molecular Weight:83.09
Yield:6086-21-1 98%
Reaction Conditions:
at 130; for 3 h;Temperature;
Steps:
2 Example III
A 1-methyl -1, 2, 4-triazole preparation method comprises: in a 500 ml flask of the three-port adding 69g1, 2, 3-triazole, then adding 234g dimethyl carbonate, raising the temperature to 130 °C reaction 3 hour; After the reaction, the reaction mixture was cooled and vacuum distilled to collect fractions at 80 ° C to obtain 40 g of 1-methyl-2-methyl-2-methyl- -1,2,4-triazole.
References:
Chongqing Tian Yi Heng Chemical Co., Ltd.;Chen, wei;Tang, yong CN105481783, 2016, A Location in patent:Paragraph 0020; 0021
288-88-0
806 suppliers
$10.00/5g
74-88-4
351 suppliers
$15.00/10g
6086-21-1
195 suppliers
$6.00/1g
10570-40-8
63 suppliers
$51.00/100mg