1-Chlorohexane synthesis
- Product Name:1-Chlorohexane
- CAS Number:544-10-5
- Molecular formula:C6H13Cl
- Molecular Weight:120.62
111-27-3
521 suppliers
$5.00/25g
544-10-5
239 suppliers
$13.00/5g
Yield:544-10-5 94.2%
Reaction Conditions:
with thionyl chloride in N,N-dimethyl-formamide at 30 - 90; for 5 h;Large scale;
Steps:
2-1 Production Example 2-1. Synthesis of 1-chlorohexane
1-hexanol (1.2 kg, 11.70 mol), DMF (8.5 g, 0.12 mol) was stirred,SOCl2 (2.1 kg, 17.6 mol) was added dropwise while maintaining an internal temperature of below 30 deg.After completion of the dropwise addition, the internal temperature was raised to 80 to 90 ° C and stirred for 5 hours.After confirming the completion of the reaction,After cooling, 5 L of purified water was added and layer separated to obtain the title compound (1.3 kg, 94.2%).
References:
KR2020/2720,2020,A Location in patent:Paragraph 0069-0071
110-54-3
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$20.00/100ml
544-10-5
239 suppliers
$13.00/5g
110-54-3
800 suppliers
$20.00/100ml
638-28-8
40 suppliers
$141.00/5g
544-10-5
239 suppliers
$13.00/5g
2346-81-8
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$267.00/10mL
6294-17-3
216 suppliers
$10.00/1g
544-10-5
239 suppliers
$13.00/5g