1-BUTYL-3-METHYLIMIDAZOLIUM NITRATE synthesis
- Product Name:1-BUTYL-3-METHYLIMIDAZOLIUM NITRATE
- CAS Number:179075-88-8
- Molecular formula:C8H15O3N3
- Molecular Weight:201.22
79917-90-1
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Yield: 96%
Reaction Conditions:
with silver nitrate in water at 60; for 1 h;
Steps:
Synthesis and characterization of BMImNO3
BMImCl (17.4 g,0.1 mol) was dissolved in distilled water (60 mL), then AgNO3 (16.9 g, 0.1 mol) was added. After stirring at 60 oC for 1 h, this mixture was filtered under reduced pressure, and filtrate was concentrated by rotary evaporation. The light yellow oil was dried at 70 oC in air, obtained in 96% yield (19.3 g).
References:
Li, Le;Li, Yu;Pang, Di;Liu, Fei;Zheng, Aqun;Zhang, Guangbin;Sun, Yang [Tetrahedron,2015,vol. 71,# 42,p. 8096 - 8103] Location in patent:supporting information
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4316-42-1
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149-73-5
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109-65-9
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179075-88-8
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1000210-73-0
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179075-88-8
132 suppliers
$68.40/5g