1,4-Dimethylcyclohexanol synthesis
- Product Name:1,4-Dimethylcyclohexanol
- CAS Number:5402-28-8
- Molecular formula:C8H16O
- Molecular Weight:128.21
Yield:5402-28-8 57%
Reaction Conditions:
Stage #1: methylmagnesium bromide in diethyl ether at 20; for 0.5 h;Schlenk technique;Inert atmosphere;
Stage #2: 1-methylcyclohexan-4-one in diethyl ether at 0 - 20; for 10 h;Schlenk technique;Inert atmosphere;
References:
Aggarwal, Varinder K.;Madhavachary, Rudrakshula;Noble, Adam;Shu, Chao [Organic Letters,2020,vol. 22,# 18,p. 7213 - 7218] Location in patent:supporting information
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