1,1-DIBROMO-1-PROPENE synthesis
- Product Name:1,1-DIBROMO-1-PROPENE
- CAS Number:13195-80-7
- Molecular formula:C3H4Br2
- Molecular Weight:199.87
Yield:13195-80-7 80%
Reaction Conditions:
Stage #1: carbon tetrabromidewith triphenylphosphine;zinc in dichloromethane at 23; for 0.5 h;Inert atmosphere;
Stage #2: acetaldehyde at 0; for 0.5 h;
References:
Newcomb, Eric T.;Knutson, Phil C.;Pedersen, Blaine A.;Ferreira, Eric M. [Journal of the American Chemical Society,2016,vol. 138,# 1,p. 108 - 111] Location in patent:supporting information
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