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Journal of Fluorine Chemistry

Journal of Fluorine Chemistry

IF: 1.7
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Fluoro-ketones VII. Synthesis of perfluoro mono- and di-ketones from perfluoro-grignard or lithium reagents and diethyl carbonate and diethyl oxalate

Published:1 November 1984 DOI: 10.1016/S0022-1139(00)80935-5
Loomis S. Chen , Grace J. Chen , Christ Tamborski

Abstract

The reaction between perfluoroalkyl-Grignard or lithium compounds and diethyl carbonate has been investigated. Under appropriate conditions, symmetric or asymmetric ketones can be prepared. The reactions of the perfluoro- Grignard or lithium compounds with diethyl oxalate can yield keto-esters and symmetric or asymmetric ketones.

Synthesis

Perfluorooctyl iodide
Diethyl carbonate
ETHYL PERFLUORONONANOATE

Substances (4)

Related products
Procduct Name CAS Molecular Formula Supplier Price
Diethyl carbonate 105-58-8 C5H10O3 515 suppliers $17.00-$2230.00
Diethyl oxalate 95-92-1 C6H10O4 476 suppliers $5.00-$1000.00
Perfluorotriethylamine 359-70-6 C6F15N 194 suppliers $20.00-$2382.77
3 5-DIMETHYOXYPHENYLMAGNESIUM CHLORIDE 89981-17-9 C8H9ClMgO2 17 suppliers $55.00-$227.00

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