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New Journal of Chemistry

New Journal of Chemistry

IF: 2.7
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Radical synthesis of trialkyl, triaryl, trisilyl and tristannyl phosphines from P4??

Published:13 April 2010 DOI: 10.1039/C0NJ00124D
Brandi M. Cossairt and Christopher C. Cummins

Abstract

A reaction scheme has been devised according to 3 RX + 3 Ti(III) + 0.25 P4 → PR3 + 3 XTi(IV), wherein RX = PhBr, CyBr, Me3SiI or Ph3SnCl, with contrasting results in the case of more hindered RX. The scheme accomplishes the direct radical functionalization of white phosphorus without the intermediacy of PCl3.

Substances (7)

Related products
Procduct Name CAS Molecular Formula Supplier Price
Pyridine hydrobromide 18820-82-1 C5H5N.BrH 376 suppliers $5.00-$4306.35
Phosphorus trichloride 7719-12-2 Cl3P 150 suppliers $30.30-$762.00
ANTIMONY (III) TELLURIDE 1327-50-0 Sb2Te3 118 suppliers $29.00-$643.65
DYNAMIN INHIBITORY PEPTIDE 251634-21-6 C47H80N18O14 51 suppliers $120.00-$840.00
Cybr antibody 14 suppliers Inquiry
CANCA 22541-14-6 H2Pr+3 9 suppliers Inquiry
CaM Kinase IV 8 suppliers Inquiry

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