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Reactive & Functional Polymers

Reactive & Functional Polymers

IF: 4.5
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4-Vinylbenzyl chloride based porous spherical polymer supports derived from water-in-oil-in-water emulsions

Published:1 November 2005 DOI: 10.1016/j.reactfunctpolym.2005.01.007
Dejan ?tefanec, Peter Krajnc

Abstract

4-Vinylbenzyl chloride (VBC) based water-in-oil-in-water emulsions with 85% pore volume and 70% VBC in organic phase were prepared and polymerised by free radical polymerisation. Porous spherical particles of diameters between 50 and 150?μm were obtained and their morphological structure and reactivity studied by FTIR spectroscopy, elemental analysis, optical microscopy, scanning electron microscopy and mercury intrusion porosimetry. Strong influence of the suspension stabiliser, namely poly(N-vinylpyrrolidone) (PVP), on the particle form was found. Diameters of spherical polymers particles depend on the PVP concentration, being larger with the lower concentration of PVP. Reactivity of novel supports was demonstrated by the reactions with piperidine, piperazine, tris(hydroxymethyl)methylamine and tris(2-aminoethyl)amine, all yielding corresponding amine derivatives.

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Related products
Procduct Name CAS Molecular Formula Supplier Price
Tris(hydroxymethyl)aminomethane 77-86-1 C4H11NO3 1142 suppliers $5.00-$8920.00
Piperazine 110-85-0 C4H10N2 628 suppliers $5.00-$1250.00
4-Vinylbenzyl chloride 1592-20-7 C9H9Cl 324 suppliers $11.00-$614.00
Tris(2-aminoethyl)amine 4097-89-6 C6H18N4 204 suppliers $10.00-$2431.28
Methacrylic acid (zirconium salt) 84057-81-8 C4H6O2.xZr 143 suppliers Inquiry
Vinylbenzyl chloride 57458-41-0 C9H9Cl 87 suppliers $56.00-$679.00

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