978-86-9

三苯甲基苯酚(978-86-9)核磁圖(¹HNMR)

產(chǎn)品名稱:三苯甲基苯酚

CAS:978-86-9

分子式:C25H20O

分子量: 336.43

InChI:InChI=1S/C25H20O/c26-24-18-16-23(17-19-24)25(20-10-4-1-5-11-20,21-12-6-2-7-13-21)22-14-8-3-9-15-22/h1-19,26H

InChIKey: NIPKXTKKYSKEON-UHFFFAOYSA-N

Smiles:C1(O)=CC=C(C(C2=CC=CC=C2)(C2=CC=CC=C2)C2=CC=CC=C2)C=C1

Mass

MS-NW-7850          
p-tritylphenol
C25H20O             (Mass of molecular ion:    336)

   Source Temperature: 200 °C
   Sample Temperature: 170 °C
   Direct, 75 eV

      51.0       1.2
      55.0       1.3
      77.0       2.1
      91.0       1.6
      94.0       1.4
     115.0       2.2
     129.0       3.2
     139.0       1.1
     151.0       1.6
     152.0       5.1
     153.0       2.9
     154.0       1.9
     164.0       1.5
     165.0      25.1
     166.0       6.0
     167.0       2.6
     168.0       2.0
     181.0      16.0
     182.0       3.9
     183.0       1.3
     189.0       1.2
     202.0       2.8
     203.0       1.2
     215.0       4.1
     216.0       1.3
     226.0       2.5
     227.0       1.7
     228.0       3.4
     229.0       2.6
     231.0       1.0
     239.0       4.2
     240.0       1.7
     241.0       3.5
     242.0       1.7
     243.0       6.8
     244.0       4.6
     257.0       5.1
     258.0       2.6
     259.0     100.0
     260.0      21.2
     261.0       2.5
     334.0       1.3
     335.0       2.1
     336.0      37.2
     337.0      10.3
     338.0       1.5

400 MHz in DMSO-d6

¹H NMR	399.65 MHz
C₂₅ H₂₀ O	0.029 g : 0.5 ml DMSO-d₆
p-tritylphenol

    Assign.     Shift(ppm)

      A             9.38
      B             7.272
      C             7.185
      D             7.130
      E             6.913
      F             6.687

     Hz     ppm     Int.

   3747.56   9.378    320
   2915.16   7.295    380
   2911.62   7.286    148
   2907.71   7.276    863
   2900.02   7.257    700
   2877.81   7.201    359
   2876.71   7.199    300
   2870.48   7.183    500
   2863.28   7.165    203
   2862.18   7.162    161
   2854.13   7.142    752
   2852.78   7.139   1000
   2845.58   7.121    755
   2844.60   7.118    727
   2770.26   6.932     50
   2767.33   6.925    337
   2765.38   6.920    143
   2762.70   6.913     48
   2760.62   6.908    137
   2758.54   6.903    428
   2755.49   6.895     58
   2679.08   6.704     60
   2675.90   6.696    410
   2673.95   6.691    152
   2671.02   6.684     46
   2669.07   6.679    122
   2667.11   6.674    354
   2664.06   6.666     45

DMSO-d6