92-54-6

N-苯基哌嗪(92-54-6)質(zhì)譜(MS)

產(chǎn)品名稱:N-苯基哌嗪

CAS:92-54-6

分子式:C10H14N2

分子量: 162.23

InChI:InChI=1S/C10H14N2/c1-2-4-10(5-3-1)12-8-6-11-7-9-12/h1-5,11H,6-9H2

InChIKey: YZTJYBJCZXZGCT-UHFFFAOYSA-N

Smiles:N1(C2=CC=CC=C2)CCNCC1

Mass

MS-NW-6038          
1-phenylpiperazine
C10H14N2            (Mass of molecular ion:    162)

   Source Temperature: 250 °C
   Sample Temperature: 190 °C
   Reservoir, 75 eV

      18.0       1.2
      27.0       2.1
      28.0       5.7
      29.0       5.2
      30.0       3.7
      39.0       1.9
      41.0       1.4
      42.0       3.0
      50.0       1.5
      51.0       5.6
      52.0       1.0
      56.0       8.8
      57.0       4.8
      65.0       1.3
      77.0      12.3
      78.0       2.1
      79.0       1.3
      81.0       1.7
      91.0       5.3
      93.0       1.0
     100.0       1.2
     104.0       9.5
     105.0      11.6
     106.0       7.1
     107.0       1.6
     118.0       1.3
     120.0     100.0
     121.0       9.3
     132.0       1.3
     162.0      32.6
     163.0       4.2

400 MHz in CDCl3

¹H NMR	399.65 MHz
C₁₀ H₁₄ N₂	0.05 ml : 0.5 ml CDCl₃
1-phenylpiperazine

    Assign.     Shift(ppm)

      A             7.237
      B             6.889
      C             6.834
      D             3.072
      E             2.949
      F             2.44

     Hz     ppm     Int.

   2900.15   7.257    518
   2899.29   7.255    290
   2898.07   7.252    209
   2896.73   7.249    223
   2895.26   7.245    128
   2892.82   7.239    643
   2891.36   7.235    692
   2889.04   7.229    142
   2886.11   7.222    215
   2884.89   7.219    240
   2884.03   7.217    594
   2758.18   6.902    525
   2757.08   6.899    688
   2755.00   6.894    302
   2750.37   6.882    332
   2749.27   6.880    582
   2748.29   6.877    582
   2739.38   6.855    180
   2738.28   6.852    286
   2737.18   6.849    177
   2731.93   6.836    241
   2730.96   6.834    451
   2730.10   6.832    266
   2724.73   6.818    139
   2723.75   6.816    231
   2722.66   6.813    146
   1233.64   3.087    750
   1228.88   3.075    904
   1226.56   3.070    628
   1223.63   3.062   1000
   1182.98   2.961    851
   1180.05   2.953    536
   1177.73   2.947    757
   1172.97   2.935    605
    976.56   2.444     92

in CDCl3