86-28-2

N-乙基咔唑(86-28-2)質(zhì)譜(MS)

產(chǎn)品名稱:N-乙基咔唑

CAS:86-28-2

分子式:C14H13N

分子量: 195.26

InChI:InChI=1S/C14H13N/c1-2-15-13-9-5-3-7-11(13)12-8-4-6-10-14(12)15/h3-10H,2H2,1H3

InChIKey: PLAZXGNBGZYJSA-UHFFFAOYSA-N

Smiles:N1(CC)C2=C(C=CC=C2)C2=C1C=CC=C2

Mass

MS-NW-2424          
9-ethylcarbazole
C14H13N             (Mass of molecular ion:    195)

   Source Temperature: 290 °C
   Sample Temperature: 170 °C
   Reservoir, 75 eV

      14.0       1.9
      18.0       3.9
      27.0       1.0
      28.0       1.1
      39.0       1.6
      40.0       1.1
      51.0       1.2
      63.0       2.3
      75.0       1.5
      76.0       1.6
      77.0       1.4
      89.0       1.1
      90.0       1.6
      97.5       2.4
     113.0       1.2
     115.0       1.2
     127.0       1.3
     139.0       3.7
     140.0       4.9
     151.0       3.4
     152.0      12.7
     153.0       3.6
     164.0       1.7
     165.0       1.3
     166.0       6.6
     167.0       3.8
     178.0       2.4
     179.0       2.6
     180.0     100.0
     181.0      14.4
     182.0       1.0
     192.0       1.3
     193.0       1.7
     194.0       3.0
     195.0      50.2
     196.0       7.9

400 MHz in CDCl3

¹H NMR	399.65 MHz
C₁₄ H₁₃ N	0.039 g : 0.5 ml CDCl₃
9-ethylcarbazole

    Assign.     Shift(ppm)

      A             8.085
      B             7.439
      C             7.368
      D             7.211
      E             4.302
      F             1.377

     Hz     ppm     Int.

   3235.96   8.097    389
   3228.27   8.078    410
   2982.67   7.464    163
   2981.57   7.461    167
   2975.59   7.446    229
   2974.49   7.443    431
   2973.39   7.440    299
   2967.41   7.426    325
   2966.31   7.423    319
   2947.75   7.376    531
   2939.58   7.356    320
   2889.77   7.231    266
   2888.67   7.229    259
   2885.74   7.221     40
   2881.84   7.211    441
   2874.88   7.194    226
   2873.90   7.192    221
   1731.08   4.332    146
   1723.75   4.314    450
   1716.55   4.296    457
   1709.35   4.278    154
    557.98   1.397    504
    550.66   1.378   1000
    543.46   1.360    512

in CDCl3