86-26-0

2-甲氧基聯(lián)苯(86-26-0)核磁圖(¹HNMR)

產(chǎn)品名稱:2-甲氧基聯(lián)苯

CAS:86-26-0

分子式:C13H12O

分子量: 184.23

InChI:InChI=1S/C13H12O/c1-14-13-10-6-5-9-12(13)11-7-3-2-4-8-11/h2-10H,1H3

InChIKey: NLWCWEGVNJVLAX-UHFFFAOYSA-N

Smiles:C1(C2=CC=CC=C2)=CC=CC=C1OC

¹HNMR

¹³CNMR

IR1

Mass

MS-NW-6036          
2-methoxybiphenyl
C13H12O             (Mass of molecular ion:    184)

   Source Temperature: 250 °C
   Sample Temperature: 190 °C
   Reservoir, 75 eV

      15.0       1.0
      39.0       4.8
      50.0       2.1
      51.0       3.9
      57.5       2.8
      62.0       1.9
      63.0       5.4
      64.0       1.5
      65.0       1.9
      69.5       1.4
      70.5       1.3
      74.0       2.0
      75.0       2.3
      76.0       4.3
      77.0       2.4
      78.0       1.1
      86.0       1.1
      87.0       1.6
      88.0       1.1
      89.0       2.8
      91.0       4.2
      92.0       1.6
     102.0       1.8
     113.0       1.5
     114.0       1.5
     115.0      19.3
     116.0       2.6
     118.0       3.6
     126.0       1.4
     127.0       1.1
     128.0       1.4
     129.0       1.0
     139.0       8.6
     140.0       2.2
     141.0      25.7
     142.0       3.6
     151.0       2.2
     152.0       5.4
     153.0       2.8
     154.0       1.4
     155.0       2.9
     156.0       1.0
     157.0       1.7
     165.0       4.0
     166.0       1.1
     167.0       2.7
     168.0       9.6
     169.0      42.8
     170.0       6.5
     181.0       1.0
     183.0      14.5
     184.0     100.0
     185.0      14.2
     186.0       1.2

400 MHz in CDCl3

¹H NMR	399.65 MHz
C₁₃ H₁₂ O	0.05 ml : 0.5 ml CDCl₃
2-methoxybiphenyl

    Assign.     Shift(ppm)

      A             7.507
      B             7.358
      C             7.29
      D             7.27
      E             7.25
      F             6.976
      G             6.900
      J             3.696

     Hz     ppm     Int.

   3005.62   7.521    200
   3004.27   7.518    251
   3002.20   7.513     78
   2997.19   7.500    280
   2996.09   7.497    243
   2994.02   7.492     49
   2948.61   7.378    115
   2947.88   7.377    160
   2946.04   7.372     62
   2940.55   7.358    310
   2939.21   7.355    153
   2934.33   7.343     97
   2932.86   7.339    179
   2930.91   7.334     38
   2916.87   7.299    134
   2915.04   7.294    166
   2913.09   7.290     90
   2911.74   7.286    143
   2910.28   7.283    106
   2909.42   7.280    156
   2907.47   7.276    248
   2904.30   7.268    169
   2902.22   7.262     59
   2899.78   7.256    137
   2899.05   7.254    134
   2898.07   7.252    131
   2897.22   7.250    143
   2895.75   7.246     50
   2891.60   7.236    110
   2889.89   7.232     90
   2795.78   6.996    103
   2794.68   6.993    104
   2788.33   6.977    175
   2787.23   6.975    178
   2780.88   6.959     85
   2779.79   6.956     83
   2762.08   6.912    158
   2761.35   6.910    149
   2753.91   6.891    144
   2753.05   6.889    137
   1477.05   3.696   1000

in CDCl3