84-85-5

4-甲氧基-1-萘酚(84-85-5)紅外圖譜(IR2)

產(chǎn)品名稱:4-甲氧基-1-萘酚

CAS:84-85-5

分子式:C11H10O2

分子量: 174.2

InChI:InChI=1S/C11H10O2/c1-13-11-7-6-10(12)8-4-2-3-5-9(8)11/h2-7,12H,1H3

InChIKey: BOTGCZBEERTTDQ-UHFFFAOYSA-N

Smiles:C1(O)=C2C(C=CC=C2)=C(OC)C=C1

Mass

MS-NW-7880          
4-methoxy-1-naphthol
C11H10O2            (Mass of molecular ion:    174)

   Source Temperature: 180 °C
   Sample Temperature: 120 °C
   Direct, 75 eV

      15.0       1.4
      18.0       1.1
      28.0       1.1
      38.0       1.0
      39.0       2.4
      50.0       4.1
      51.0       7.3
      52.0       1.5
      53.0       1.8
      57.5       1.0
      62.0       2.2
      63.0       4.3
      65.0       1.7
      65.5       2.0
      74.0       3.0
      75.0       4.5
      76.0       6.9
      77.0      19.6
      78.0       1.6
      86.0       1.4
      87.0       5.0
      88.0       1.6
      89.0       2.2
      91.0       3.8
     101.0       2.3
     102.0       7.9
     103.0      18.1
     104.0       4.3
     105.0      13.3
     106.0       2.1
     113.0       1.5
     114.0       1.9
     115.0       5.9
     116.0       1.0
     129.0       1.0
     130.0       3.2
     131.0      23.8
     132.0       2.5
     145.0       3.1
     159.0     100.0
     160.0      11.6
     161.0       1.1
     173.0       5.8
     174.0      85.5
     175.0      10.8
     176.0       1.0

400 MHz in DMSO-d6

¹H NMR	399.65 MHz
C₁₁ H₁₀ O₂	0.039 g : 0.5 ml DMSO-d₆
4-methoxy-1-naphthol

    Assign.     Shift(ppm)

      A             9.59
      B     *1      8.12
      C     *1      8.09
      D     *2      7.498
      E     *2      7.479
      F             6.790
      G             6.772
      J             3.883
     
     J(F,G)=8.2HZ

     Hz     ppm     Int.

   3834.53   9.595    378
   3252.56   8.139     65
   3251.95   8.137     69
   3248.90   8.130     86
   3246.77   8.125     51
   3245.09   8.120     68
   3242.95   8.115     79
   3242.19   8.113     84
   3239.75   8.107     84
   3238.98   8.105     70
   3236.85   8.100     69
   3235.17   8.096     53
   3233.03   8.090     99
   3229.98   8.083     86
   3229.37   8.081     68
   2997.44   7.501    202
   2994.69   7.494    113
   2993.62   7.491    106
   2991.49   7.486    114
   2990.57   7.483     99
   2987.67   7.476    191
   2720.18   6.807     65
   2712.10   6.787    303
   2707.82   6.776    258
   2699.58   6.755     58
   1551.82   3.883   1000

KBr disc