1HNMR)的核磁圖,紅外圖譜,Raman光譜,質(zhì)譜等圖譜" /> 1HNMR)" />

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75-77-4

三甲基氯硅烷(75-77-4)核磁圖(1HNMR)

產(chǎn)品名稱:三甲基氯硅烷

CAS:75-77-4

分子式:C3H9ClSi

分子量: 108.64

InChI:InChI=1S/C3H9ClSi/c1-5(2,3)4/h1-3H3

InChIKey: IJOOHPMOJXWVHK-UHFFFAOYSA-N

Smiles:[Si](Cl)(C)(C)C

  • 圖譜
    Mass 

    MS-NW-3310          
chlorotrimethylsilane
C3H9ClSi            (Mass of molecular ion:    108)


       Source Temperature: 280 °C
   Sample Temperature: 180 °C
   Reservoir, 75 eV


          28.0       1.4
      29.0       2.1
      42.0       2.1
      43.0       6.7
      44.0       2.0
      45.0       4.8
      53.0       1.6
      55.0       1.0
      63.0      10.2
      64.0       1.4
      65.0      12.2
      67.0       3.6
      72.0       2.6
      73.0      35.2
      74.0       3.0
      75.0       1.6
      77.0       1.3
      78.0       1.4
      79.0       2.5
      92.0       1.0
      93.0     100.0
      94.0       7.8
      95.0      35.4
      96.0       2.5
      97.0       1.2
     108.0       3.6
     110.0       1.2
     147.0       2.1

parameter in CCl4

90 MHz in CDCl3

  • 圖譜

    1H NMR 300 MHz
    C3 H9 Cl Si 5 vol% in CCl4
    chlorotrimethylsilane
    ChemicalStructure 
        Parameter     ppm  Hz
    
      D(A)         0.42
     
     SCHMIDBAUR,H. J.AM.CHEM.SOC. 85, 2336 (1963)
     J(C-13,A):120.5HZ. J(SI-29,A):7.10HZ.
  

         Hz     ppm     Int.


        126.00   0.420   1000

  • 圖譜

    1H NMR 89.56 MHz
    C3 H9 Cl Si 0.04 ml : 0.5 ml CDCl3
    chlorotrimethylsilane
    ChemicalStructure 
        Assign.     Shift(ppm)
    
      A             0.431
     
     J(SI-29,A)=7.0HZ.
  

         Hz     ppm     Int.


         42.13   0.471     45
     38.63   0.432   1000
     35.13   0.393     48

in CDCl3

  • 圖譜

liquid film

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