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75-03-6

碘乙烷(75-03-6)質(zhì)譜(MS)

產(chǎn)品名稱:碘乙烷

CAS:75-03-6

分子式:C2H5I

分子量: 155.97

InChI:InChI=1S/C2H5I/c1-2-3/h2H2,1H3

InChIKey: HVTICUPFWKNHNG-UHFFFAOYSA-N

Smiles:CCI

  • 圖譜
    Mass 

    MS-NW-0530          
iodoethane
C2H5I               (Mass of molecular ion:    156)


       Source Temperature: 280 °C
   Sample Temperature: 170 °C
   Reservoir, 75 eV


          26.0       7.1
      27.0      57.5
      28.0       7.4
      29.0      99.9
      30.0       2.4
     127.0      16.8
     128.0       5.4
     141.0       1.8
     156.0     100.0
     157.0       2.2

90 MHz in CDCl3

parameter in CDCl3

  • 圖譜

    1H NMR 89.56 MHz
    C2 H5 I 0.04 ml : 0.5 ml CDCl3
    iodoethane
    ChemicalStructure 
        Assign.     Shift(ppm)
    
      A             3.186
      B             1.847
     
     J(A,B)=7.6HZ
  

         Hz     ppm     Int.


        297.69   3.324     92
    297.00   3.317     93
    289.81   3.236    341
    282.94   3.160    221
    282.31   3.153    404
    275.31   3.075    133
    274.69   3.068    127
    172.38   1.925    406
    165.19   1.845   1000
    164.75   1.840    593
    157.50   1.759    311

  • 圖譜

    1H NMR 300 MHz
    C2 H5 I 10 vol% in CCl4
    iodoethane
    ChemicalStructure 
        Parameter     ppm  Hz
    
      D(A)         1.859
      D(B)         3.155
       J(A,B)          7.446
     
     EBERSOLE,S. ET AL. J.PHYS.CHEM. 68, 3430 (1964)
  

         Hz     ppm     Int.


        957.78   3.193    152
    950.32   3.168    472
    942.88   3.143    489
    935.45   3.118    170
    565.08   1.884    509
    557.64   1.859   1000
    550.19   1.834    467

in CDCl3

  • 圖譜

CCl4 solution

  • 圖譜

liquid film

  • 圖譜

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