碘甲烷(74-88-4)質(zhì)譜(MS)
InChI:InChI=1S/CH3I/c1-2/h1H3
InChIKey: INQOMBQAUSQDDS-UHFFFAOYSA-N
Smiles:CI
-
Mass
MS2014-05092CW
iodomethane
CH3I (Mass of molecular ion: 142)
Source Temperature: 250 °C
Sample Temperature: 250 °C
Reservoir, 70 eV
15.0 4.3
28.0 4.7
32.0 1.2
94.0 1.2
96.0 1.2
127.0 26.8
128.0 1.7
139.0 4.1
140.0 3.6
141.0 13.1
142.0 100.0
143.0 1.1
parameter in CCl4
in CDCl3
parameter in CDCl3
-
| 1H NMR |
300 MHz |
| C H3 I
|
10 wt% in CCl4
|
| iodomethane
|
 |
Parameter ppm Hz
D(A) 2.162
LACEY,M.J. ET AL. AUST.J.CHEM. 23, 1421 (1970)
J(GEM):-9.355HZ DETERMINED IN NEAT LIQUID. J(C-13,H):151.0HZ.
|
Hz ppm Int.
648.60 2.162 1000
-
-
| 1H NMR |
300 MHz |
| C H3 I
|
0.05 ml : 0.5 ml CDCl3
|
| iodomethane
|
|
Parameter ppm Hz
D(A) 2.165
|
Hz ppm Int.
649.50 2.165 1000
PHOTOLYSIS, ON SILICA GEL
CH3 RADICAL, PHOTOLYSIS OF 13CH3I(50%)-VYCOR GLASS
METHYL RADICAL, PHOTOLYSIS, ON SILICA GEL
IO RADICAL, REACTION OF O ATOM
CH3 RADICAL, PHOTOLYSIS, ON VYCOR GLASS
METHYL RADICAL, X-IRRAD.(53%13C), 77K