683-18-1

二丁基二氯化錫(683-18-1)核磁圖(¹³CNMR)

產(chǎn)品名稱:二丁基二氯化錫

CAS:683-18-1

分子式:C8H18Cl2Sn

分子量: 303.84

InChI:InChI=1S/2C4H9.2ClH.Sn/c2*1-3-4-2;;;/h2*1,3-4H2,2H3;2*1H;/q;;;;+2/p-2

InChIKey: RJGHQTVXGKYATR-UHFFFAOYSA-L

Smiles:[Sn](CCCC)(CCCC)(Cl)Cl

Mass

MS2017-05432CM      
dibutyltin dichloride
C8H18Cl2Sn          (Mass of molecular ion:    304)

   Source Temperature: 250 °C
   Sample Temperature:  20 °C
   Direct, 70 eV

      18.0       1.5
      27.0       4.2
      28.0       2.4
      29.0      17.6
      39.0       3.7
      41.0      22.0
      42.0       1.4
      55.0       2.4
      56.0       3.7
      57.0     100.0
      58.0       4.3
     117.0       1.1
     118.0       1.2
     119.0       1.6
     120.0       1.6
     121.0       1.8
     151.0       4.8
     152.0       2.6
     153.0       9.4
     154.0       3.6
     155.0      13.1
     156.0       1.0
     157.0       4.9
     159.0       2.4
     177.0       1.0
     190.0       1.4
     208.0       4.6
     209.0       3.8
     210.0       8.8
     211.0       5.6
     212.0      11.7
     213.0       2.4
     214.0       4.3
     216.0       2.1
     243.0       4.0
     244.0       2.3
     245.0       8.9
     246.0       4.0
     247.0      13.2
     248.0       2.3
     249.0       7.4
     251.0       3.2
     253.0       1.2
     265.0       1.6
     266.0       2.1
     267.0       2.9
     268.0       3.1
     269.0       3.5
     270.0       1.3
     271.0       1.3

90 MHz in CDCl3

¹H NMR	89.56 MHz
C₈ H₁₈ Cl₂ Sn	0.043 g : 0.5 ml CDCl₃
dibutyltin dichloride

    Assign.     Shift(ppm)

      A             0.96
      B             1.3
      C             1.5
      D             1.80

     Hz     ppm     Int.

    168.13   1.878     47
    166.13   1.855    247
    164.38   1.836    112
    162.19   1.811   1000
    159.94   1.786    253
    159.50   1.781    282
    158.69   1.772    236
    157.69   1.761    179
    156.44   1.747    135
    153.56   1.715     65
    152.69   1.705     51
    149.63   1.671     41
    148.31   1.656     43
    146.94   1.641     30
    145.81   1.629     37
    145.25   1.622     38
    144.50   1.614     48
    143.25   1.600     54
    139.63   1.560     52
    139.06   1.553     54
    136.25   1.522     67
    135.25   1.511     78
    134.75   1.505     74
    134.13   1.498     70
    133.25   1.488     88
    132.63   1.481     94
    131.56   1.469    107
    130.25   1.455     91
    129.31   1.444     83
    127.38   1.423    104
    125.50   1.402    116
    124.25   1.388     87
    123.63   1.381    121
    121.13   1.353     80
    119.63   1.336     83
    119.06   1.330     67
    117.50   1.312     96
    116.06   1.296     71
    114.63   1.280     48
    113.13   1.264     40
    110.81   1.238     39
     93.13   1.040    217
     92.13   1.029    420
     88.81   0.992     39
     85.81   0.959    798
     79.38   0.887    122
     78.25   0.874    194
     76.56   0.855    111

in CDCl3