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637-60-5

4-甲基苯肼鹽酸鹽(637-60-5)質(zhì)譜(MS)

產(chǎn)品名稱(chēng):4-甲基苯肼鹽酸鹽

CAS:637-60-5

分子式:C7H11ClN2

分子量: 158.63

InChI:InChI=1S/C7H10N2.ClH/c1-6-2-4-7(9-8)5-3-6;/h2-5,9H,8H2,1H3;1H

InChIKey: HMHWNJGOHUYVMD-UHFFFAOYSA-N

Smiles:N(C1=CC=C(C)C=C1)N.[H]Cl

  • 圖譜
    Mass 

    MS-NW-0632          
p-tolylhydrazine hydrochloride
C7H10N2 HCl         (Mass of molecular ion:    122)


       Source Temperature: 200 °C
   Sample Temperature: 160 °C
   Direct, 75 eV


          17.0       1.3
      18.0       5.2
      26.0       1.2
      27.0       5.3
      28.0       4.2
      29.0       3.2
      31.0       1.6
      35.0       5.7
      36.0      32.8
      37.0       1.9
      38.0      10.4
      39.0      12.0
      40.0       1.5
      41.0       3.4
      43.0       1.2
      50.0       6.1
      51.0      12.5
      52.0       8.1
      53.0       5.1
      54.0       1.1
      61.0       1.2
      62.0       2.6
      63.0       6.3
      64.0       2.3
      65.0      12.7
      66.0       1.8
      67.0       1.2
      74.0       1.0
      75.0       1.0
      76.0       1.6
      77.0      36.1
      78.0      16.6
      79.0      40.0
      80.0       3.6
      89.0       3.1
      90.0       1.8
      91.0      24.5
      92.0       9.4
      93.0       3.5
      94.0       1.6
     104.0       8.9
     105.0       7.1
     106.0      56.9
     107.0      12.5
     120.0       2.1
     121.0       9.4
     122.0     100.0
     123.0       8.5

90 MHz in D2O

  • 圖譜

    1H NMR 89.56 MHz
    C7 H10 N2 0.043 g : 0.5 ml D2O
    p-tolylhydrazine hydrochloride
    ChemicalStructure 
        Assign.     Shift(ppm)
    
      A             7.26
      B             7.04
      C             4.83
      D             2.311
     
     C-PEAK INCLUDES H2O.
  

         Hz     ppm     Int.


        656.19   7.327     75
    655.81   7.323     76
    647.56   7.231    159
    635.50   7.096     49
    633.25   7.071    202
    631.06   7.047     57
    626.69   6.998     47
    624.63   6.975     93
    432.31   4.828   1000
    207.00   2.312    444

in D2O

  • 圖譜

KBr disc

  • 圖譜

nujol mull

  • 圖譜

  • 圖譜

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