4-Methylphenylhydrazine hydrochloride(637-60-5) MS

Product Name4-Methylphenylhydrazine hydrochloride

CAS 637-60-5

Molecular FormulaC7H11ClN2

Molecular Weight158.63

InChIInChI=1S/C7H10N2.ClH/c1-6-2-4-7(9-8)5-3-6;/h2-5,9H,8H2,1H3;1H

InChIKey HMHWNJGOHUYVMD-UHFFFAOYSA-N

SmilesN(C1=CC=C(C)C=C1)N.[H]Cl

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4-Methylphenylhydrazine hydrochloride(637-60-5) MS
Mass

MS-NW-0632          
p-tolylhydrazine hydrochloride
C7H10N2 HCl         (Mass of molecular ion:    122)

   Source Temperature: 200 °C
   Sample Temperature: 160 °C
   Direct, 75 eV

      17.0       1.3
      18.0       5.2
      26.0       1.2
      27.0       5.3
      28.0       4.2
      29.0       3.2
      31.0       1.6
      35.0       5.7
      36.0      32.8
      37.0       1.9
      38.0      10.4
      39.0      12.0
      40.0       1.5
      41.0       3.4
      43.0       1.2
      50.0       6.1
      51.0      12.5
      52.0       8.1
      53.0       5.1
      54.0       1.1
      61.0       1.2
      62.0       2.6
      63.0       6.3
      64.0       2.3
      65.0      12.7
      66.0       1.8
      67.0       1.2
      74.0       1.0
      75.0       1.0
      76.0       1.6
      77.0      36.1
      78.0      16.6
      79.0      40.0
      80.0       3.6
      89.0       3.1
      90.0       1.8
      91.0      24.5
      92.0       9.4
      93.0       3.5
      94.0       1.6
     104.0       8.9
     105.0       7.1
     106.0      56.9
     107.0      12.5
     120.0       2.1
     121.0       9.4
     122.0     100.0
     123.0       8.5

90 MHz in D2O

4-Methylphenylhydrazine hydrochloride(637-60-5) MS

¹H NMR	89.56 MHz
C₇ H₁₀ N₂	0.043 g : 0.5 ml D₂O
p-tolylhydrazine hydrochloride

    Assign.     Shift(ppm)

      A             7.26
      B             7.04
      C             4.83
      D             2.311
     
     C-PEAK INCLUDES H2O.

     Hz     ppm     Int.

    656.19   7.327     75
    655.81   7.323     76
    647.56   7.231    159
    635.50   7.096     49
    633.25   7.071    202
    631.06   7.047     57
    626.69   6.998     47
    624.63   6.975     93
    432.31   4.828   1000
    207.00   2.312    444

in D2O