13CNMR)的核磁圖,紅外圖譜,Raman光譜,質譜等圖譜" /> 13CNMR)" />

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62-73-7

敵敵畏(62-73-7)核磁圖(13CNMR)

產品名稱:敵敵畏

CAS:62-73-7

分子式:C4H7Cl2O4P

分子量: 220.98

InChI:InChI=1S/C4H7Cl2O4P/c1-8-11(7,9-2)10-3-4(5)6/h3H,1-2H3

InChIKey: OEBRKCOSUFCWJD-UHFFFAOYSA-N

Smiles:P(OC)(OC)(O/C=C(/Cl)\Cl)=O

  • 圖譜
    Mass 

    MS-NW-8751          
2,2-dichlorovinyl dimethyl phosphate
C4H7Cl2O4P          (Mass of molecular ion:    220)


       Source Temperature: 260 °C
   Sample Temperature: 140 °C
   Reservoir, 75 eV


          15.0      13.0
      28.0       1.1
      29.0       2.0
      31.0       2.7
      47.0       6.3
      48.0       1.6
      49.0       1.2
      50.0       1.0
      60.0       1.5
      76.0       2.8
      78.0       1.1
      79.0      17.6
      83.0       2.3
      85.0       1.4
      93.0       2.5
      95.0       1.7
      97.0       2.2
     109.0     100.0
     110.0       3.1
     111.0       1.3
     113.0       2.3
     145.0       6.2
     147.0       2.0
     185.0      18.3
     187.0       6.0
     220.0       4.0
     222.0       2.6

in CDCl3

90 MHz in CDCl3

  • 圖譜

  • 圖譜

    1H NMR 89.56 MHz
    C4 H7 Cl2 O4 P 0.05 ml : 0.5 ml CDCl3
    2,2-dichlorovinyl dimethyl phosphate
    ChemicalStructure 
        Assign.     Shift(ppm)
    
      A             6.998
      B             3.868
     
     J(P-31,A)=5.2HZ. J(P-31,B)=11.4HZ.
  

         Hz     ppm     Int.


        629.38   7.028    208
    624.13   6.969    210
    352.13   3.932   1000
    349.50   3.903     25
    348.56   3.892     23
    343.88   3.840     27
    340.75   3.805    990
    338.19   3.777     23

in CDCl3

  • 圖譜

liquid film

  • 圖譜

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