613-42-3

4-芐基聯(lián)苯(613-42-3)核磁圖(¹HNMR)

產(chǎn)品名稱:4-芐基聯(lián)苯

CAS:613-42-3

分子式:C19H16

分子量: 244.33

InChI:InChI=1S/C19H16/c1-3-7-16(8-4-1)15-17-11-13-19(14-12-17)18-9-5-2-6-10-18/h1-14H,15H2

InChIKey: AGPLQTQFIZBOLI-UHFFFAOYSA-N

Smiles:C1(C2=CC=CC=C2)=CC=C(CC2=CC=CC=C2)C=C1

Mass

MS-NW-1268          
4-benzylbiphenyl
C19H16              (Mass of molecular ion:    244)

   Source Temperature: 260 °C
   Sample Temperature: 180 °C
   Reservoir, 75 eV

      39.0       2.0
      51.0       2.1
      63.0       1.8
      65.0       2.1
      77.0       1.7
      78.0       1.1
      89.0       1.5
      91.0       8.1
     115.0       4.8
     122.0       1.3
     128.0       1.2
     139.0       1.3
     141.0       1.6
     151.0       1.0
     152.0       5.1
     153.0       3.1
     164.0       1.2
     165.0      18.9
     166.0       9.4
     167.0      16.8
     168.0       2.3
     202.0       1.6
     203.0       1.0
     215.0       2.8
     216.0       1.1
     226.0       1.0
     227.0       1.2
     228.0       4.4
     229.0       5.5
     230.0       1.0
     239.0       2.2
     240.0       1.0
     241.0       3.3
     242.0       1.8
     243.0      18.6
     244.0     100.0
     245.0      20.4
     246.0       2.0

400 MHz in CDCl3

¹H NMR	399.65 MHz
C₁₉ H₁₆	11.6 mg : 0.5 ml CDCl₃
4-benzylbiphenyl

    Assign.     Shift(ppm)

      A             7.564
      B             7.512
      C             7.413
      D             7.32
      E             7.30
      F             7.26
      G             7.22
      J             7.21
      K             4.021

     Hz     ppm     Int.

   3028.81   7.579    381
   3027.47   7.576    470
   3025.51   7.571    156
   3022.22   7.563    162
   3021.36   7.561    228
   3020.39   7.558    546
   3019.65   7.556    404
   3019.17   7.555    528
   3017.21   7.550    113
   3015.50   7.546     49
   3014.16   7.543     42
   3013.79   7.542     41
   3011.84   7.537     41
   3008.91   7.529     83
   3006.84   7.524    550
   3004.88   7.519    231
   3000.49   7.508    222
   2998.41   7.503    694
   2996.46   7.498    143
   2994.02   7.492     46
   2993.04   7.490     42
   2991.33   7.485     32
   2972.78   7.439     78
   2971.80   7.437    193
   2971.07   7.435    303
   2969.24   7.430    132
   2967.53   7.426     43
   2966.67   7.424     40
   2965.70   7.421    106
   2965.09   7.420    132
   2963.75   7.416    572
   2962.40   7.413    274
   2959.23   7.405     50
   2957.52   7.401    172
   2955.93   7.397    328
   2955.44   7.396    298
   2953.86   7.392     85
   2950.44   7.383     32
   2940.80   7.359     34
   2932.86   7.339    144
   2931.64   7.336    262
   2930.30   7.333    167
   2928.96   7.329     45
   2927.25   7.325    141
   2926.27   7.323    288
   2924.19   7.317    329
   2922.12   7.312    132
   2919.80   7.306    319
   2918.58   7.303    401
   2917.97   7.302    376
   2916.87   7.299    255
   2915.65   7.296    143
   2913.57   7.291    169
   2911.62   7.286    436
   2910.89   7.284    344
   2909.79   7.281    158
   2906.98   7.274    123
   2904.91   7.269    597
   2904.42   7.268    507
   2902.95   7.264    233
   2900.88   7.259     82
   2898.44   7.253    198
   2897.09   7.250    428
   2896.48   7.248    550
   2893.68   7.241    289
   2891.60   7.236   1000
   2889.77   7.231    368
   2887.82   7.226    152
   2886.84   7.224    181
   2886.35   7.223    191
   2885.62   7.221    261
   2885.01   7.219    344
   2884.40   7.218    339
   2883.67   7.216    374
   2881.59   7.211    269
   2879.39   7.205     97
   2878.17   7.202     67
   2875.85   7.196     82
   2874.51   7.193    103
   2873.54   7.191     57
   2873.05   7.189     61
   1606.93   4.021    866
   1599.12   4.002     30

in CDCl3