610-49-1

1-氨基蒽(610-49-1)質(zhì)譜(MS)

產(chǎn)品名稱:1-氨基蒽

CAS:610-49-1

分子式:C14H11N

分子量: 193.24

InChI:InChI=1S/C14H11N/c15-14-7-3-6-12-8-10-4-1-2-5-11(10)9-13(12)14/h1-9H,15H2

InChIKey: YUENFNPLGJCNRB-UHFFFAOYSA-N

Smiles:C1(N)=C2C(C=C3C(=C2)C=CC=C3)=CC=C1

Mass

MS-NW-6213          
1-anthrylamine
C14H11N             (Mass of molecular ion:    193)

   Source Temperature: 250 °C
   Sample Temperature: 190 °C
   Reservoir, 75 eV

      17.0       1.9
      18.0       8.5
      39.0       1.7
      44.0       2.1
      50.0       1.8
      51.0       2.9
      52.0       2.3
      53.0       1.1
      60.0       1.2
      62.0       1.3
      63.0       2.4
      65.0       1.5
      66.0       3.5
      69.5       1.9
      74.0       1.5
      75.0       1.7
      76.0       2.5
      77.0       3.4
      78.0       2.7
      79.0       1.4
      81.0       1.2
      81.5       2.6
      82.0       4.2
      82.5       5.7
      83.0       2.1
      83.5       2.7
      86.0       1.0
      87.0       1.3
      88.0       1.9
      89.0       2.2
      95.5       4.0
      96.0       1.2
      96.5      11.0
      97.0       2.4
     104.0       7.9
     105.0       4.5
     115.0       1.8
     131.0      10.4
     132.0      36.2
     133.0       3.6
     139.0       2.7
     140.0       1.3
     141.0       1.0
     150.0       1.1
     151.0       1.4
     152.0       2.0
     153.0       1.4
     163.0       4.0
     164.0       3.9
     165.0      24.7
     166.0       7.1
     167.0       1.6
     176.0       2.7
     177.0       2.2
     178.0       9.6
     179.0       2.2
     190.0       2.8
     191.0       3.7
     192.0       8.6
     193.0     100.0
     194.0      20.8
     195.0       6.6
     196.0       1.0

90 MHz in CDCl3

¹H NMR	89.56 MHz
C₁₄ H₁₁ N	0.044 g : 0.5 ml CDCl₃
1-anthrylamine

    Assign.     Shift(ppm)

      A             8.30
      B             7.91
      C          7.56 to 7.27
      D             7.32
      E             7.21
      F             6.657
      G             4.00
     
     CONFIRMED BY LAOCN PROGRAM.

     Hz     ppm     Int.

    743.44   8.302   1000
    716.50   8.001     62
    713.81   7.971    229
    710.63   7.935    230
    707.56   7.901    254
    704.56   7.867    293
    704.00   7.861    301
    701.44   7.833    101
    699.25   7.808     38
    672.19   7.506    134
    671.38   7.497    140
    671.00   7.493    145
    670.50   7.487    149
    669.13   7.472     95
    668.31   7.463     82
    666.56   7.443    561
    663.75   7.412    492
    662.88   7.402    459
    660.50   7.375    229
    659.50   7.364    219
    656.63   7.332    584
    654.88   7.313    452
    652.88   7.290     73
    650.06   7.259     35
    648.00   7.236    460
    646.44   7.218    160
    639.50   7.141    221
    600.06   6.701    310
    598.81   6.687    280
    593.13   6.623    254
    591.88   6.609    229
    357.81   3.996    170

in CDCl3