586-77-6

4-溴-N,N-二甲基苯胺(586-77-6)Raman光譜

產(chǎn)品名稱:4-溴-N,N-二甲基苯胺

CAS:586-77-6

分子式:C8H10BrN

分子量: 200.08

InChI:InChI=1S/C8H10BrN/c1-10(2)8-5-3-7(9)4-6-8/h3-6H,1-2H3

InChIKey: XYZWMVYYUIMRIZ-UHFFFAOYSA-N

Smiles:C1(N(C)C)=CC=C(Br)C=C1

Mass

MS-NW-4324          
p-bromo-N,N-dimethylaniline
C8H10BrN            (Mass of molecular ion:    199)

   Source Temperature: 230 °C
   Sample Temperature: 180 °C
   Reservoir, 75 eV

      15.0       5.9
      27.0       2.0
      28.0       1.2
      37.0       1.9
      38.0       4.0
      39.0       4.8
      41.0       1.8
      42.0      14.5
      43.0       2.0
      44.0       3.8
      50.0      10.8
      51.0       7.9
      51.5       3.5
      52.0       4.0
      53.0       1.1
      58.5       4.3
      59.5       4.0
      60.0       2.0
      61.0       1.2
      62.0       2.3
      63.0       8.1
      64.0       2.9
      65.0       2.0
      66.0       1.3
      68.0       1.1
      73.0       1.2
      74.0       4.9
      75.0       8.5
      76.0       9.2
      77.0      15.0
      78.0       6.9
      79.0       3.0
      89.0       1.2
      90.0       4.2
      91.0       4.3
      91.5       1.2
      92.0       3.6
      92.5       1.1
      99.0       1.5
      99.5       4.5
     100.0       1.9
     100.5       4.0
     104.0      10.7
     105.0      10.1
     117.0       1.2
     118.0      23.9
     119.0       8.3
     120.0       2.4
     155.0       6.4
     156.0       1.1
     157.0       6.1
     158.0       1.1
     182.0       6.9
     183.0      12.0
     184.0       9.5
     185.0      12.3
     186.0       2.7
     196.0       1.0
     198.0      94.7
     199.0      96.4
     200.0     100.0
     201.0      91.8
     202.0       8.4

90 MHz in CDCl3

¹H NMR	89.56 MHz
C₈ H₁₀ Br N	0.050 g : 0.5 ml CDCl₃
p-bromo-N,N-dimethylaniline

    Assign.     Shift(ppm)

      A             7.28
      B             6.58
      C             2.907

     Hz     ppm     Int.

    657.38   7.341    107
    655.06   7.315     35
    650.50   7.264     34
    648.19   7.238    159
    592.94   6.621     96
    590.63   6.595     29
    586.06   6.544     22
    583.75   6.518     75
    260.31   2.907   1000

in CDCl3