5317-33-9

1-(3-羥丙基)-4-甲基哌嗪(5317-33-9)質(zhì)譜(MS)

產(chǎn)品名稱:1-(3-羥丙基)-4-甲基哌嗪

CAS:5317-33-9

分子式:C8H18N2O

分子量: 158.24

¹HNMR

¹³CNMR

IR1

Mass

MS-IW-0870          
3-(4-methyl-1-piperazinyl)-1-propanol
C8H18N2O            (Mass of molecular ion:    158)

   Source Temperature: 220 °C
   Sample Temperature: 150 °C
   Reservoir, 75 eV

      15.0       1.4
      18.0       1.4
      27.0       1.8
      28.0       5.1
      29.0       2.0
      30.0       3.1
      31.0       3.2
      41.0       3.3
      42.0      17.9
      43.0      49.3
      44.0      16.8
      54.0       1.4
      55.0       2.3
      56.0      12.8
      57.0      11.4
      58.0      17.2
      59.0       3.1
      70.0      58.8
      71.0      16.4
      72.0       4.7
      82.0       1.3
      84.0       3.7
      85.0       7.5
      86.0       1.5
      87.0       4.0
      88.0       4.2
      97.0       1.4
      98.0       8.0
      99.0       4.2
     100.0       7.1
     101.0       1.0
     102.0       2.9
     111.0       1.6
     113.0     100.0
     114.0      10.0
     127.0       1.6
     157.0       1.1
     158.0      46.3
     159.0       5.2

400 MHz in CDCl3

¹H NMR	399.65 MHz
C₈ H₁₈ N₂ O	0.05 ml : 0.5 ml CDCl₃
3-(4-methyl-1-piperazinyl)-1-propanol

    Assign.     Shift(ppm)

      A             5.1
      B             3.732
      C             2.574
      D             2.5
      E             2.276
      F             1.719

     Hz     ppm     Int.

   2045.78   5.119     22
   1497.44   3.747    253
   1491.82   3.733    348
   1486.21   3.719    262
   1035.03   2.590    254
   1028.69   2.574    429
   1022.34   2.559    278
    925.90   2.317     21
    923.46   2.311     22
    920.41   2.304     25
    909.91   2.277   1000
    896.85   2.245     27
    699.10   1.750     63
    692.99   1.734    168
    686.89   1.719    205
    681.40   1.705    164
    675.29   1.690     63

in CDCl3