1HNMR)的核磁圖,紅外圖譜,Raman光譜,質(zhì)譜等圖譜" /> 1HNMR)" />

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53-70-3

二苯并[a,h]蒽(53-70-3)核磁圖(1HNMR)

產(chǎn)品名稱:二苯并[a,h]蒽

CAS:53-70-3

分子式:C22H14

分子量: 278.35

InChI:InChI=1S/C22H14/c1-3-7-19-15(5-1)9-11-17-14-22-18(13-21(17)19)12-10-16-6-2-4-8-20(16)22/h1-14H

InChIKey: LHRCREOYAASXPZ-UHFFFAOYSA-N

Smiles:C12=CC=CC=C1C=CC1C2=CC2C(=C3C=CC=CC3=CC=2)C=1

  • 圖譜
    Mass 

    MS-NW-0121          
dibenz(a,H)anthracene
C22H14              (Mass of molecular ion:    278)


       Source Temperature:   0 °C
   Sample Temperature:   0 °C
   Direct, 75 eV


          18.0       1.1
      28.0       1.4
     112.0       1.2
     113.0       1.3
     124.0       1.4
     125.0       3.1
     126.0       1.8
     137.0       3.2
     137.5       1.2
     138.0       6.7
     138.5       2.0
     139.0      12.2
     139.5       3.0
     248.0       1.1
     250.0       2.0
     252.0       1.2
     274.0       4.9
     275.0       2.3
     276.0      17.1
     277.0       6.0
     278.0     100.0
     279.0      23.9
     280.0       3.0

400 MHz in CDCl3

90 MHz in CDCl3

  • 圖譜

    1H NMR 399.65 MHz
    C22 H14 saturated in CDCl3
    dibenz(a,h)anthracene
    ChemicalStructure 
        Assign.     Shift(ppm)
    
      A             9.155
      B             8.875
      C             7.962
      D             7.918
      E             7.763
      F     *1      7.722
      G     *1      7.653
     
     J(B,F)=8.1HZ. J(C,E)=8.9HZ. J(D,G)=7.8HZ.
  

         Hz     ppm     Int.


       3658.69   9.155   1000
   3652.47   9.140     37
   3651.86   9.138     30
   3555.91   8.898     34
   3555.42   8.897     36
   3555.18   8.896     36
   3554.69   8.895     34
   3551.39   8.887    370
   3546.88   8.875     53
   3543.33   8.867    380
   3540.04   8.858     63
   3539.06   8.856     51
   3537.60   8.852     32
   3191.04   7.985     42
   3187.13   7.975    550
   3183.84   7.967     61
   3182.98   7.965     65
   3181.88   7.962     77
   3178.22   7.953    700
   3175.29   7.946     98
   3174.56   7.944    103
   3174.07   7.943     95
   3173.22   7.940     74
   3171.88   7.937     57
   3169.19   7.930    370
   3167.85   7.927    378
   3165.28   7.921    107
   3161.38   7.911    432
   3160.03   7.907    440
   3157.35   7.901     79
   3155.15   7.895     51
   3110.96   7.785     38
   3110.35   7.783     41
   3109.86   7.782     40
   3106.57   7.774    654
   3103.64   7.766     75
   3103.15   7.765     67
   3102.78   7.764     66
   3101.68   7.761     73
   3100.46   7.758     69
   3100.22   7.758     69
   3097.66   7.751    549
   3094.85   7.744    271
   3093.38   7.741    278
   3091.43   7.736     74
   3091.06   7.735     71
   3090.09   7.732     58
   3089.72   7.732     62
   3087.77   7.727    371
   3086.43   7.723    454
   3085.21   7.720    294
   3082.76   7.714     70
   3082.52   7.714     70
   3081.91   7.712     68
   3079.71   7.707    352
   3078.13   7.703    340
   3075.44   7.696     55
   3075.07   7.695     54
   3074.10   7.692     47
   3073.73   7.692     50
   3073.12   7.690     42
   3072.75   7.689     39
   3070.92   7.685     39
   3070.56   7.684     38
   3070.19   7.683     39
   3069.34   7.681     38
   3065.43   7.671    400
   3064.09   7.667    425
   3061.28   7.660     54
   3060.42   7.658     55
   3058.23   7.653    350
   3057.62   7.651    460
   3056.40   7.648    413
   3052.61   7.639     65
   3050.54   7.634    248
   3049.32   7.630    227
   3047.49   7.626     35

  • 圖譜

    1H NMR 89.56 MHz
    C22 H14 0.008 g : 0.5 ml CDCl3
    dibenz(a,h)anthracene
    ChemicalStructure 
        Assign.     Shift(ppm)
    
      A             9.144
      B             8.86
      C             7.94
      D             7.90
      E             7.76
      F             7.72
      G             7.63
  

         Hz     ppm     Int.


        819.06   9.146    937
    799.06   8.923    195
    798.50   8.916    191
    797.94   8.910    146
    796.38   8.893    193
    793.06   8.856    125
    792.50   8.849    122
    790.31   8.825    221
    789.75   8.819    248
    789.44   8.815    244
    717.88   8.016    294
    716.81   8.004    118
    713.50   7.967    203
    711.63   7.946    188
    709.00   7.917    748
    707.38   7.899    323
    706.94   7.894    311
    704.25   7.864    401
    700.25   7.819    152
    698.00   7.794    730
    695.88   7.770    130
    693.31   7.742    460
    691.06   7.717    326
    690.13   7.706    556
    689.00   7.694    335
    687.06   7.672   1000
    683.06   7.627    469
    681.25   7.607    306

KBr disc

  • 圖譜

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  • 圖譜

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