alpha-四氫萘酚(529-33-9)核磁圖(13CNMR)
InChI:InChI=1S/C10H12O/c11-10-7-3-5-8-4-1-2-6-9(8)10/h1-2,4,6,10-11H,3,5,7H2
InChIKey: JAAJQSRLGAYGKZ-UHFFFAOYSA-N
Smiles:C1(O)C2=C(C=CC=C2)CCC1
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Mass
MS-NW-7392
1,2,3,4-tetrahydro-1-naphthol
C10H12O (Mass of molecular ion: 148)
Source Temperature: 210 °C
Sample Temperature: 190 °C
Reservoir, 75 eV
17.0 1.1
18.0 5.2
27.0 1.8
28.0 1.0
38.0 1.2
39.0 5.2
41.0 1.1
50.0 4.7
51.0 11.4
52.0 2.2
61.0 1.0
62.0 2.3
63.0 8.9
63.5 3.4
64.0 11.8
64.5 2.9
65.0 5.8
74.0 3.6
75.0 3.4
76.0 2.9
77.0 7.7
78.0 3.9
87.0 1.1
89.0 3.5
90.0 2.1
91.0 8.9
92.0 1.8
98.0 1.0
101.0 2.3
102.0 5.4
103.0 2.3
104.0 2.4
105.0 3.8
115.0 40.9
116.0 5.0
117.0 1.4
118.0 2.6
119.0 6.0
120.0 10.7
121.0 1.1
126.0 4.2
127.0 17.6
128.0 40.0
129.0 77.7
130.0 100.0
131.0 11.7
132.0 1.2
146.0 1.9
147.0 4.9
148.0 5.0
90 MHz in CDCl3
400 MHz in CDCl3
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| 1H NMR |
89.56 MHz |
| C10 H12 O
|
0.04 ml : 0.5 ml CDCl3
|
| 1,2,3,4-tetrahydro-1-naphthol
|
 |
Assign. Shift(ppm)
A 7.38
B 7.28 to 6.96
C 4.72
D 2.74
E 2.02
F 2.14 to 1.47
|
Hz ppm Int.
666.94 7.447 128
665.38 7.430 76
664.75 7.423 107
663.94 7.414 117
662.56 7.398 194
661.88 7.391 269
660.19 7.372 88
658.19 7.350 316
654.75 7.311 134
650.81 7.267 69
649.81 7.256 89
647.13 7.226 530
643.19 7.182 523
641.50 7.163 782
640.44 7.151 266
639.25 7.138 380
638.00 7.124 1000
636.63 7.109 532
635.88 7.101 515
634.94 7.090 372
633.88 7.078 183
632.38 7.061 195
631.81 7.055 172
631.25 7.049 163
629.94 7.034 89
628.63 7.020 59
627.13 7.003 64
626.25 6.993 73
427.19 4.770 146
426.56 4.763 143
425.81 4.755 127
423.19 4.726 245
422.81 4.721 244
419.19 4.681 146
253.81 2.834 88
253.38 2.830 93
251.06 2.804 219
249.31 2.784 162
246.75 2.756 352
244.88 2.735 362
240.75 2.689 228
240.31 2.684 223
236.63 2.643 65
186.00 2.077 95
184.81 2.064 123
180.56 2.017 681
177.56 1.983 281
175.75 1.963 375
174.81 1.952 448
173.69 1.940 391
172.81 1.930 335
171.75 1.918 478
170.06 1.899 587
169.50 1.893 628
168.75 1.885 669
166.19 1.856 462
164.88 1.842 378
163.94 1.831 398
163.56 1.827 398
159.25 1.779 134
158.94 1.775 137
158.19 1.767 144
155.94 1.742 107
155.19 1.733 119
153.56 1.715 92
152.81 1.707 123
152.19 1.700 104
151.56 1.693 120
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| 1H NMR |
399.65 MHz |
| C10 H12 O
|
0.020 g : 0.5 ml CDCl3
|
| 1,2,3,4-tetrahydro-1-naphthol
|
|
Assign. Shift(ppm)
A 7.419
B 7.21 to 7.18
C 7.099
D 4.765
E *1 2.81
F *1 2.72
G 2.05 to 1.92
J *2 1.89
K 1.84
L *2 1.77
|
Hz ppm Int.
2970.09 7.432 278
2966.67 7.424 295
2965.58 7.421 299
2963.87 7.417 187
2963.13 7.415 171
2960.94 7.409 351
2884.89 7.219 87
2883.67 7.216 68
2880.25 7.207 933
2877.56 7.201 441
2876.34 7.198 522
2875.12 7.195 438
2873.90 7.192 564
2871.09 7.185 1000
2869.02 7.179 83
2868.41 7.178 78
2867.80 7.176 84
2866.58 7.173 130
2840.94 7.109 325
2838.75 7.104 158
2838.13 7.102 162
2836.55 7.098 267
2835.45 7.095 231
2832.15 7.087 205
1904.91 4.767 235
1135.99 2.843 102
1130.62 2.830 70
1124.76 2.815 147
1119.14 2.801 247
1114.26 2.789 165
1100.59 2.754 107
1094.60 2.739 150
1093.02 2.735 191
1089.84 2.727 67
1087.40 2.721 129
1086.91 2.720 128
1084.96 2.715 64
1078.25 2.698 79
1077.27 2.696 87
1076.66 2.695 89
1076.05 2.693 88
801.51 2.006 109
800.90 2.005 93
798.95 2.000 159
798.22 1.998 170
797.00 1.995 248
795.41 1.991 121
794.31 1.988 210
791.63 1.981 337
790.28 1.978 175
789.55 1.976 204
786.87 1.969 468
783.57 1.961 172
781.98 1.957 198
780.88 1.954 220
779.30 1.950 146
778.20 1.948 167
777.34 1.946 118
776.86 1.944 131
776.00 1.942 157
773.44 1.936 166
771.85 1.932 138
770.63 1.929 105
769.53 1.926 141
768.19 1.923 174
766.24 1.918 103
764.53 1.913 95
763.18 1.910 152
762.33 1.908 199
761.11 1.905 186
757.93 1.897 117
756.96 1.895 78
755.37 1.891 179
754.88 1.889 167
753.05 1.885 124
752.20 1.883 101
751.10 1.880 160
750.49 1.878 151
745.36 1.866 101
744.75 1.864 89
733.15 1.835 341
725.10 1.815 77
724.12 1.812 94
720.95 1.804 122
714.60 1.789 186
711.43 1.781 194
709.35 1.775 118
708.25 1.773 175
705.69 1.766 150
704.22 1.763 106
702.39 1.758 85
700.68 1.754 67
699.71 1.751 89
698.36 1.748 110
697.63 1.746 101
697.27 1.745 108
692.38 1.733 65