辛基三氯硅烷(5283-66-9)紅外圖譜(IR1)
分子式:C8H17Cl3Si
分子量: 247.66
InChI:InChI=1S/C8H17Cl3Si/c1-2-3-4-5-6-7-8-12(9,10)11/h2-8H2,1H3
InChIKey: RCHUVCPBWWSUMC-UHFFFAOYSA-N
Smiles:C([Si](Cl)(Cl)Cl)CCCCCCC
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Mass
MS-NW-3330
trichlorooctylsilane
C8H17Cl3Si (Mass of molecular ion: 246)
Source Temperature: 280 °C
Sample Temperature: 180 °C
Reservoir, 75 eV
27.0 8.8
28.0 2.1
29.0 14.7
39.0 6.8
40.0 1.3
41.0 24.9
42.0 11.8
43.0 100.0
44.0 3.2
53.0 1.5
54.0 1.3
55.0 13.4
56.0 12.4
57.0 48.7
58.0 2.4
63.0 2.0
65.0 1.0
69.0 4.1
70.0 4.3
71.0 25.9
72.0 1.6
84.0 2.1
85.0 40.4
86.0 2.9
98.0 1.4
99.0 1.7
100.0 1.1
101.0 1.1
117.0 1.1
125.0 1.5
127.0 1.1
133.0 14.9
135.0 15.0
137.0 5.0
139.0 2.9
141.0 2.2
153.0 2.8
155.0 1.8
161.0 5.3
163.0 5.0
165.0 1.7
167.0 2.2
169.0 1.3
174.0 1.7
175.0 13.0
176.0 3.0
177.0 13.4
178.0 1.8
179.0 4.8
189.0 4.6
190.0 1.1
191.0 4.1
193.0 1.4
203.0 3.7
204.0 1.0
205.0 3.4
207.0 1.3
217.0 2.2
219.0 2.3
246.0 1.2
248.0 1.2
90 MHz in CDCl3
400 MHz in CDCl3
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| 1H NMR |
89.56 MHz |
| C8 H17 Cl3 Si
|
0.04 ml : 0.5 ml CDCl3
|
| trichlorooctylsilane
|
 |
Assign. Shift(ppm)
A 1.76 to 1.08
B 0.89
|
Hz ppm Int.
154.25 1.723 36
153.94 1.719 39
153.31 1.712 39
152.56 1.704 39
152.19 1.700 41
151.88 1.696 43
151.25 1.689 43
150.56 1.682 47
148.75 1.661 62
148.44 1.658 62
147.88 1.652 63
147.56 1.648 61
146.25 1.633 70
145.88 1.629 70
145.38 1.624 73
144.50 1.614 77
143.44 1.602 85
141.25 1.578 113
134.94 1.507 252
129.63 1.448 496
127.06 1.419 372
126.75 1.416 368
125.63 1.403 367
115.88 1.294 997
115.19 1.287 1000
104.19 1.164 39
103.00 1.151 37
102.44 1.144 36
102.06 1.140 36
84.63 0.945 167
79.31 0.886 549
73.25 0.818 114
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| 1H NMR |
399.65 MHz |
| C8 H17 Cl3 Si
|
0.05 ml : 0.5 ml CDCl3
|
| trichlorooctylsilane
|
|
Assign. Shift(ppm)
A 1.58
B 1.48 to 1.360
C 1.36 to 1.210
D 0.89
|
Hz ppm Int.
648.68 1.624 51
647.09 1.620 50
643.31 1.610 61
641.60 1.606 127
639.04 1.599 104
636.96 1.594 95
634.89 1.589 136
633.30 1.585 191
632.45 1.583 180
630.00 1.577 101
628.66 1.574 110
627.32 1.570 136
625.37 1.565 199
622.19 1.557 121
620.48 1.553 61
617.68 1.546 105
616.46 1.543 100
584.72 1.464 31
576.54 1.443 78
576.05 1.442 79
574.71 1.439 82
569.21 1.425 179
564.94 1.414 606
562.01 1.407 271
559.69 1.401 333
556.88 1.394 348
555.79 1.391 380
548.83 1.374 288
548.22 1.372 292
544.19 1.362 64
543.58 1.361 64
530.52 1.328 215
523.68 1.311 381
518.68 1.298 545
517.21 1.295 569
515.14 1.289 655
512.94 1.284 728
365.72 0.916 60
361.33 0.905 342
354.61 0.888 1000
347.53 0.870 379