1HNMR)的核磁圖,紅外圖譜,Raman光譜,質(zhì)譜等圖譜" /> 1HNMR)" />

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返回ChemicalBook首頁(yè)>CAS數(shù)據(jù)庫(kù)列表>41830-80-2更多圖譜> 5,9-二氨基苯并[A]吩惡嗪-7-高氯酸鹽(41830-80-2)核磁圖(1HNMR)

41830-80-2

5,9-二氨基苯并[A]吩惡嗪-7-高氯酸鹽(41830-80-2)核磁圖(1HNMR)

分子式:C16H12ClN3O5

分子量: 361.74

  • 圖譜
    Mass

    MS-NW-7464          
    cresyl violet perchlorate
    C16H12ClN3O5        (Mass of molecular ion:    361)
    

       Source Temperature: 230 °C
       Sample Temperature: 250 °C
       Direct, 75 eV
    

          17.0       2.9
          18.0      12.9
          28.0       4.8
          35.0       1.2
          36.0       8.6
          38.0       2.9
          39.0       2.5
          41.0       2.4
          44.0      12.8
          50.0       1.0
          51.0       1.9
          52.0       2.6
          62.0       1.4
          63.0       3.3
          64.0       2.3
          65.0       1.4
          66.0       2.0
          67.0       1.9
          75.0       1.5
          76.0       2.4
          77.0       1.2
          78.0       1.6
          79.0       2.7
          80.0       1.0
          87.0       1.0
          88.0       1.2
          89.0       2.1
          89.5       1.1
          90.0       1.1
          91.0       2.8
         102.0       1.6
         102.5       1.1
         103.0       2.7
         104.0       1.0
         113.0       1.7
         114.0       1.0
         117.0      12.5
         117.5       2.3
         121.0       2.3
         128.0       1.1
         130.0       1.1
         130.5       3.5
         139.0       1.0
         140.0       1.5
         151.0       1.1
         177.0       1.0
         178.0       1.4
         179.0       1.3
         205.0       5.8
         206.0       2.0
         232.0       1.6
         233.0       2.1
         234.0      20.3
         235.0       4.4
         260.0       9.2
         261.0     100.0
         262.0      19.2
         263.0       2.2
         287.0       2.6
    

400 MHz in DMSO-d6

  • 圖譜

    1H NMR 399.65 MHz
    C16 H12 Cl N3 O5 0.046 g : 0.5 ml DMSO-d6
    cresyl violet perchlorate
    ChemicalStructure
        Assign.     Shift(ppm)
    A *1 9.70 B *1 9.61 C *2 8.503 D *2 8.269 E 7.87 F *3 7.836 G *3 7.738 J 7.601 K 6.956 L 6.581 M 6.580

         Hz     ppm     Int.
    

       3876.80   9.701     60
       3839.57   9.608     57
       3403.02   8.516    197
       3401.95   8.513    199
       3394.93   8.495    221
       3393.86   8.493    208
       3309.02   8.280    177
       3300.78   8.260    193
       3100.43   7.758    128
       3099.21   7.755    129
       3092.19   7.738    190
       3091.13   7.735    146
       3085.17   7.720     95
       3083.95   7.717     91
       3042.76   7.614    439
       3033.75   7.592    494
       2785.95   6.971    207
       2783.66   6.966    205
       2776.95   6.949    198
       2774.66   6.943    210
       2631.38   6.585    540
       2629.85   6.581   1000
    

KBr disc

  • 圖譜

nujol mull

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