三乙酰氧基乙烯基硅烷(4130-08-9)核磁圖(13CNMR)
分子式:C8H12O6Si
分子量: 232.26
InChI:InChI=1S/C8H12O6Si/c1-5-15(12-6(2)9,13-7(3)10)14-8(4)11/h5H,1H2,2-4H3
InChIKey: NOZAQBYNLKNDRT-UHFFFAOYSA-N
Smiles:[Si](OC(=O)C)(OC(=O)C)(OC(=O)C)C=C
-
Mass
MS-NW-8335
triacetoxyvinylsilane
C8H12O6Si (Mass of molecular ion: 232)
Source Temperature: 260 °C
Sample Temperature: 140 °C
Reservoir, 75 eV
13.0 1.1
14.0 4.1
15.0 16.9
16.0 1.8
27.0 1.7
28.0 7.5
29.0 3.2
41.0 1.7
42.0 11.2
43.0 89.7
44.0 3.0
45.0 34.6
60.0 22.5
61.0 1.3
62.0 5.3
63.0 14.8
76.0 4.5
79.0 30.1
80.0 1.6
81.0 1.2
87.0 2.9
88.0 3.0
89.0 39.9
90.0 3.2
91.0 1.8
102.0 1.3
103.0 1.2
104.0 5.1
105.0 2.5
118.0 1.0
120.0 1.0
121.0 100.0
122.0 7.6
123.0 5.6
129.0 1.1
130.0 11.1
131.0 51.5
132.0 5.4
133.0 4.4
139.0 1.2
146.0 1.5
147.0 5.7
148.0 3.6
149.0 2.2
163.0 55.5
164.0 5.4
165.0 2.9
167.0 1.1
172.0 7.2
173.0 9.2
174.0 1.5
175.0 3.1
177.0 1.5
189.0 3.7
190.0 1.3
191.0 1.1
205.0 35.5
206.0 4.3
207.0 2.1
209.0 3.6
217.0 1.7
218.0 3.0
219.0 2.6
251.0 4.2
260.0 2.0
261.0 2.0
293.0 3.6
303.0 2.2
335.0 3.5
90 MHz in CDCl3
parameter in CDCl3
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| 1H NMR |
89.56 MHz |
| C8 H12 O6 Si
|
0.04 ml : 0.5 ml CDCl3
|
| triacetoxyvinylsilane
|
 |
Assign. Shift(ppm)
A 6.38 to 6.04
B 2.161
|
Hz ppm Int.
570.06 6.366 37
562.13 6.277 71
558.56 6.237 88
555.44 6.202 80
547.50 6.114 39
193.56 2.162 1000
189.88 2.121 41
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| 1H NMR |
300 MHz |
| C8 H12 O6 Si
|
0.05 ml : 0.5 ml CDCl3
|
| triacetoxyvinylsilane
|
|
Parameter ppm Hz
D(A) 6.344
D(B) 6.224
D(C) 6.110
J(A,B) 3.0
J(A,C) 15.4
J(B,C) 18.6
D(D) 2.163
|
Hz ppm Int.
1913.35 6.378 21
1909.33 6.364 23
1898.96 6.330 29
1894.94 6.316 38
1880.78 6.269 12
1876.80 6.256 17
1862.21 6.207 50
1858.23 6.194 34
1846.32 6.154 51
1831.89 6.106 31
1827.75 6.092 16
1813.36 6.045 13
648.91 2.163 1000