369-36-8

2-氟-5-硝基苯胺(369-36-8)紅外圖譜(IR2)

產品名稱:2-氟-5-硝基苯胺

CAS:369-36-8

分子式:C6H5FN2O2

分子量: 156.11

InChI:InChI=1S/C6H5FN2O2/c7-5-2-1-4(9(10)11)3-6(5)8/h1-3H,8H2

InChIKey: KJVBJICWGQIMOZ-UHFFFAOYSA-N

Smiles:C1(N)=CC([N+]([O-])=O)=CC=C1F

Mass

MS-NW-9430          
2-fluoro-5-nitroaniline
C6H5FN2O2           (Mass of molecular ion:    156)

   Source Temperature: 250 °C
   Sample Temperature: 160 °C
   Reservoir, 75 eV

      18.0       3.3
      28.0       5.8
      30.0       1.9
      31.0       2.6
      33.0       1.6
      37.0       1.3
      38.0       2.6
      39.0       6.5
      41.0       1.4
      50.0       1.7
      51.0       4.1
      52.0       4.8
      56.0       1.9
      57.0      16.8
      58.0       1.1
      59.0       1.8
      61.0       2.0
      62.0       3.8
      63.0      19.0
      64.0       2.9
      65.0       2.0
      70.0       2.3
      71.0       1.9
      72.0       1.0
      76.0       1.0
      78.0       1.6
      80.0       1.0
      81.0       5.8
      82.0       7.7
      83.0      53.6
      84.0       7.1
      89.0       2.3
      90.0      37.9
      91.0       2.9
      97.0       1.1
      98.0      16.4
      99.0       1.1
     106.0       1.4
     108.0       1.3
     109.0       6.0
     110.0      56.0
     111.0       4.3
     126.0      11.8
     140.0       1.2
     156.0     100.0
     157.0       7.7

400 MHz in CDCl3

¹H NMR	399.65 MHz
C₆ H₅ F N₂ O₂	0.044 g : 0.5 ml CDCl₃
2-fluoro-5-nitroaniline

    Assign.     Shift(ppm)

      A             7.667
      B             7.591
      C             7.085
      D             4.12

     Hz     ppm     Int.

   3069.70   7.681    734
   3067.02   7.675    872
   3062.13   7.663    753
   3059.33   7.656    870
   3041.75   7.612    469
   3038.94   7.605    488
   3037.72   7.601    554
   3034.79   7.594    455
   3032.84   7.589    552
   3030.03   7.582    549
   3028.81   7.579    587
   3026.00   7.572    449
   2845.46   7.120     28
   2840.58   7.108    827
   2831.54   7.086    957
   2830.57   7.083   1000
   2821.53   7.061    762
   1646.48   4.120    530

in CDCl3