3562-73-0

1-(4-聯(lián)聯(lián)苯基)乙醇(3562-73-0)質(zhì)譜(MS)

產(chǎn)品名稱(chēng):1-(4-聯(lián)聯(lián)苯基)乙醇

CAS:3562-73-0

分子式:C14H14O

分子量: 198.26

InChI:InChI=1S/C14H14O/c1-11(15)12-7-9-14(10-8-12)13-5-3-2-4-6-13/h2-11,15H,1H3

InChIKey: GOISDOCZKZYADO-UHFFFAOYSA-N

Smiles:C1(=CC=C(C(O)C)C=C1)C1=CC=CC=C1

Mass

MS2016-05336CW      
1-(4-biphenylyl)ethanol
C14H14O             (Mass of molecular ion:    198)

   Source Temperature: 240 °C
   Sample Temperature:  20 °C
   Direct, 70 eV

      43.0       8.4
      51.0       3.0
      63.0       2.2
      75.0       1.7
      76.0       6.4
      77.0      13.9
      78.0       1.7
      88.0       1.2
      89.0       2.7
      91.0       1.1
      91.5       8.5
      99.0       2.3
     102.0       1.8
     115.0       5.2
     121.0       1.6
     126.0       2.1
     127.0       4.6
     128.0       4.1
     129.0       3.6
     139.0       1.5
     150.0       2.0
     151.0       6.4
     152.0      23.1
     153.0      17.8
     154.0      15.3
     155.0      95.6
     156.0      12.4
     165.0       7.6
     166.0       2.6
     167.0       2.1
     176.0       1.7
     177.0       1.3
     178.0       8.2
     179.0       6.5
     180.0      21.6
     181.0      12.7
     182.0       3.0
     183.0     100.0
     184.0      13.8
     185.0       1.1
     196.0       2.6
     197.0       3.8
     198.0      63.5
     199.0       9.6

400 MHz in CDCl3

in DMSO-d6

¹H NMR	399.65 MHz
C₁₄ H₁₄ O	0.039 g : 0.5 ml CDCl₃
1-(4-biphenylyl)ethanol

    Assign.     Shift(ppm)

      A             7.57
      B             7.56
      C             7.42
      D             7.41
      E             7.331
      F             4.904
      G             2.12
      J             1.506

     Hz     ppm     Int.

   3029.42   7.581    230
   3028.08   7.577    313
   3026.12   7.572    133
   3024.41   7.568    365
   3022.34   7.563    270
   3021.00   7.560    357
   3019.78   7.557    321
   3017.94   7.552    199
   3015.99   7.547    505
   3014.04   7.542     96
   2973.75   7.441     53
   2972.90   7.439    121
   2972.05   7.437    190
   2970.21   7.433     83
   2968.38   7.428     91
   2966.55   7.423    486
   2964.84   7.419    494
   2963.50   7.416    215
   2959.96   7.407    133
   2958.50   7.403    425
   2957.03   7.400    272
   2955.08   7.395     64
   2936.77   7.349     83
   2935.55   7.346    153
   2934.20   7.342     89
   2930.18   7.332     64
   2928.10   7.327    174
   2926.03   7.322     52
   2922.12   7.312     42
   2920.78   7.309     72
   2919.56   7.306     39
   1969.60   4.929     40
   1963.13   4.913    121
   1956.79   4.897    124
   1950.32   4.881     43
    847.29   2.121    116
    605.35   1.515    980
    598.88   1.499   1000
    595.21   1.490     30