34732-09-7

2,3,4-三氯苯磺酰氯(34732-09-7)核磁圖(¹HNMR)

產(chǎn)品名稱:2,3,4-三氯苯磺酰氯

CAS:34732-09-7

分子式:C6H2Cl4O2S

分子量: 279.96

InChI:InChI=1S/C6H2Cl4O2S/c7-3-1-2-4(13(10,11)12)6(9)5(3)8/h1-2H

InChIKey: JDAJYNHGBUXIKS-UHFFFAOYSA-N

Smiles:C1(S(Cl)(=O)=O)=CC=C(Cl)C(Cl)=C1Cl

Mass

MS-NW-6868          
2,3,4-trichlorobenzenesulfonyl chloride
C6H2Cl4O2S          (Mass of molecular ion:    278)

   Source Temperature: 140 °C
   Sample Temperature: 120 °C
   Direct, 75 eV

      18.0       2.4
      28.0       2.0
      35.0       2.1
      36.0       3.4
      37.0       4.7
      38.0       1.5
      44.0       1.1
      45.0       1.1
      47.0       1.5
      48.0       5.8
      49.0       2.3
      50.0       2.4
      54.0       1.7
      60.0       1.2
      61.0       3.9
      62.0       2.6
      64.0       6.8
      69.0       1.6
      71.0       1.7
      71.5       3.7
      72.0       5.0
      72.5       2.8
      73.0      10.8
      74.0      24.9
      75.0       2.0
      79.0       1.6
      83.0       2.1
      84.0      11.8
      85.0       2.7
      86.0       4.1
      96.0       1.6
      97.0       3.7
      99.0       1.2
     106.0       1.1
     107.0       4.3
     108.0      17.2
     109.0      22.7
     110.0       6.7
     111.0       7.1
     118.0       2.9
     119.0       2.2
     120.0       2.0
     121.0       1.3
     121.5       2.1
     122.5       2.3
     131.0       1.0
     143.0      25.6
     144.0      14.8
     145.0      18.7
     146.0       9.4
     147.0       3.7
     148.0       1.6
     160.0       1.0
     167.0       4.2
     169.0       3.9
     171.0       1.3
     176.0       1.1
     178.0       1.4
     179.0      66.6
     180.0       8.6
     181.0      66.0
     182.0       7.1
     183.0      21.6
     184.0       2.2
     185.0       2.5
     195.0      15.3
     196.0       1.1
     197.0      15.2
     198.0       1.1
     199.0       5.6
     201.0       1.4
     214.0       6.9
     216.0       8.9
     218.0       4.5
     220.0       1.0
     227.0       1.3
     229.0       1.3
     243.0     100.0
     244.0       7.4
     245.0      98.0
     246.0       7.5
     247.0      34.5
     248.0       2.7
     249.0       4.9
     278.0      28.9
     279.0       2.1
     280.0      38.6
     281.0       3.1
     282.0      19.5
     283.0       1.5
     284.0       4.7
     288.0       1.1
     290.0       1.5
     358.0       1.4
     360.0       2.5
     362.0       1.9

parameter in CDCl3

400 MHz in CDCl3

¹H NMR	300 MHz
C₆ H₂ Cl₄ O₂ S	0.038 g : 0.5 ml CDCl₃
2,3,4-trichlorobenzenesulfonyl chloride

    Parameter     ppm  Hz

      D(A)         8.032
      D(B)         7.637
       J(A,B)          8.75

     Hz     ppm     Int.

   2414.13   8.047    863
   2405.39   8.018   1000
   2295.32   7.651   1000
   2286.57   7.622    863

¹H NMR	399.65 MHz
C₆ H₂ Cl₄ O₂ S	0.041 g : 0.5 ml CDCl₃
2,3,4-trichlorobenzenesulfonyl chloride

    Assign.     Shift(ppm)

      A             8.041
      B             7.645

     Hz     ppm     Int.

   3218.26   8.053    907
   3209.47   8.031   1000
   3059.69   7.656    990
   3050.90   7.634    892

in CDCl3

KBr disc

nujol mull

更多供應商

Capot Chemical Co., Ltd

Clearsynth Labs Limited

安徽科迪達化工有限公司

九鼎化學（上海）科技有限公司

山東小野化學股份有限公司

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2,3,4-三氯苯磺酰氯(34732-09-7)核磁圖(1HNMR)

2,3,4-三氯苯磺酰氯(34732-09-7)核磁圖(¹HNMR)