1-氟萘(321-38-0)Raman光譜
InChI:InChI=1S/C10H7F/c11-10-7-3-5-8-4-1-2-6-9(8)10/h1-7H
InChIKey: CWLKTJOTWITYSI-UHFFFAOYSA-N
Smiles:C1(F)=C2C(C=CC=C2)=CC=C1
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Mass
MS-NW-5447
1-fluoronaphthalene
C10H7F (Mass of molecular ion: 146)
Source Temperature: 260 °C
Sample Temperature: 190 °C
Reservoir, 75 eV
50.0 2.3
51.0 1.7
60.0 2.5
62.0 1.3
63.0 2.2
72.0 1.3
73.0 5.7
74.0 2.8
75.0 3.5
94.0 1.7
96.0 1.8
98.0 1.1
99.0 2.4
120.0 6.1
125.0 5.6
126.0 3.8
127.0 1.0
144.0 3.2
145.0 7.2
146.0 100.0
147.0 11.1
90 MHz in CDCl3
400 MHz in CDCl3
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| 1H NMR |
89.56 MHz |
| C10 H7 F
|
0.04 ml : 0.5 ml CDCl3
|
| 1-fluoronaphthalene
|
 |
Assign. Shift(ppm)
A 8.08
B 7.80
C 7.55
D *1 7.50
E *1 7.48
G 7.31
J 7.11
|
Hz ppm Int.
729.50 8.146 130
726.75 8.115 126
726.13 8.108 151
724.56 8.091 101
723.88 8.083 100
723.19 8.075 69
722.44 8.067 94
721.50 8.057 73
719.88 8.038 187
706.13 7.885 67
705.75 7.881 70
705.38 7.877 70
705.00 7.872 66
704.00 7.861 76
703.19 7.852 98
701.63 7.835 107
699.50 7.811 167
697.50 7.789 136
696.19 7.774 133
695.81 7.770 127
694.38 7.754 137
692.44 7.732 57
684.31 7.641 115
683.88 7.637 130
683.44 7.632 155
682.44 7.620 128
678.88 7.581 101
678.00 7.571 99
676.19 7.551 276
674.88 7.536 1000
672.06 7.505 302
671.25 7.495 395
668.88 7.469 319
668.06 7.460 410
666.56 7.443 48
665.31 7.429 612
662.56 7.398 229
660.44 7.375 353
655.06 7.315 305
652.38 7.285 197
646.94 7.224 192
645.50 7.208 251
643.94 7.191 242
638.06 7.125 120
636.44 7.107 104
634.88 7.089 235
633.56 7.075 235
627.38 7.006 129
626.06 6.991 122
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| 1H NMR |
399.65 MHz |
| C10 H7 F
|
0.05 ml : 0.5 ml CDCl3
|
| 1-fluoronaphthalene
|
|
Assign. Shift(ppm)
A 8.09
B 7.80
C 7.564
D *1 7.49
E *1 7.47
G 7.331
J 7.103
J(F-19,G) = 5.4 HZ.
J(F-19,J) = 10.7 HZ.
J(G,J)= 7.7 HZ.
J(C,J)= 1.0 HZ.
J(C,G) = 8.3 HZ.
|
Hz ppm Int.
3242.68 8.114 31
3240.36 8.108 71
3237.30 8.101 347
3235.11 8.095 240
3233.03 8.090 305
3227.66 8.077 403
3124.39 7.818 66
3121.95 7.812 230
3120.24 7.808 344
3118.65 7.804 209
3116.70 7.799 255
3115.11 7.795 293
3112.92 7.790 355
3110.72 7.784 275
3107.18 7.775 72
3027.59 7.576 567
3019.29 7.555 678
3010.38 7.533 30
3006.59 7.524 41
3004.52 7.518 40
3000.98 7.510 98
2998.90 7.504 192
2994.14 7.492 626
2992.55 7.488 870
2988.53 7.478 1000
2984.50 7.468 715
2983.03 7.465 677
2978.27 7.453 188
2976.20 7.448 100
2973.39 7.440 33
2973.02 7.440 33
2972.17 7.437 34
2940.31 7.358 325
2934.94 7.344 339
2932.50 7.338 463
2927.12 7.325 461
2924.44 7.318 342
2918.95 7.304 318
2848.02 7.127 369
2847.05 7.124 403
2840.33 7.108 335
2839.36 7.105 363
2837.28 7.100 396
2836.30 7.097 414
2829.59 7.081 317
2828.74 7.079 344