3182-95-4

L-苯丙氨醇(3182-95-4)Raman光譜

產(chǎn)品名稱:L-苯丙氨醇

CAS:3182-95-4

分子式:C9H13NO

分子量: 151.21

InChI:InChI=1/C9H13NO/c10-9(7-11)6-8-4-2-1-3-5-8/h1-5,9,11H,6-7,10H2/t9-/s3

InChIKey: STVVMTBJNDTZBF-DJEYLCQNNA-N

Smiles:C(C1C=CC=CC=1)[C@H](N)CO |&1:7,r|

Mass

MS-NW-6201          
L-2-amino-3-phenyl-1-propanol
C9H13NO             (Mass of molecular ion:    151)

   Source Temperature: 260 °C
   Sample Temperature: 190 °C
   Reservoir, 75 eV

      15.0       1.6
      18.0       1.4
      28.0       3.3
      30.0       3.6
      31.0       1.3
      39.0       3.0
      41.0       1.4
      42.0      14.7
      43.0       1.9
      50.0       1.0
      51.0       2.5
      59.0       1.2
      59.5       1.2
      60.0     100.0
      61.0       2.7
      63.0       1.6
      65.0       4.4
      77.0       5.1
      78.0       1.2
      89.0       1.1
      91.0      12.7
      92.0       3.1
      93.0       1.9
     103.0       7.4
     104.0       1.5
     117.0       1.3
     118.0       1.9
     119.0       1.3
     120.0      33.0
     121.0       3.2

400 MHz in CDCl3

¹H NMR	399.65 MHz
C₉ H₁₃ N O	0.039 g : 0.5 ml CDCl₃
L-2-amino-3-phenyl-1-propanol

    Assign.     Shift(ppm)

      A             7.287
      B             7.20
      C             7.19
      D     *1      3.591
      E     *1      3.374
      F             3.093
      G     *2      2.777
      J     *2      2.513
      K             2.4
     
     J(D,E)=-10.6HZ
     J(D,F)=4.0HZ
     J(E,F)=7.2HZ
     J(F,G)=5.3HZ
     J(F,J)=8.5HZ
     J(G,J)=-13.4HZ

     Hz     ppm     Int.

   2922.12   7.312    236
   2921.14   7.310    343
   2919.56   7.306    182
   2915.89   7.297    318
   2914.06   7.292    864
   2910.64   7.283    131
   2908.08   7.277    351
   2906.74   7.274    775
   2888.92   7.229    173
   2887.57   7.226    354
   2886.23   7.222    323
   2878.91   7.204   1000
   2877.44   7.200    975
   2875.12   7.195    229
   2874.39   7.193    225
   2870.73   7.184    735
   1443.24   3.612    381
   1439.21   3.602    401
   1432.62   3.585    487
   1428.59   3.575    473
   1357.18   3.396    426
   1349.98   3.378    488
   1346.44   3.370    353
   1339.36   3.352    392
   1248.41   3.124    105
   1244.38   3.114    125
   1243.16   3.111    147
   1241.21   3.106    139
   1239.75   3.103    188
   1239.26   3.101    188
   1237.30   3.096    143
   1235.96   3.093    259
   1234.62   3.090    171
   1232.67   3.085    178
   1230.71   3.080    155
   1228.76   3.075    133
   1227.54   3.072    134
   1223.51   3.062    103
   1120.12   2.803    260
   1114.87   2.790    246
   1106.69   2.770    336
   1101.44   2.757    305
   1015.01   2.540    374
   1006.47   2.519    367
   1001.59   2.507    322
    993.04   2.485    306

in CDCl3