2909-79-7

4-叔丁基-N,N-二甲基苯胺(2909-79-7)質(zhì)譜(MS)

產(chǎn)品名稱:4-叔丁基-N,N-二甲基苯胺

CAS:2909-79-7

分子式:C12H19N

分子量: 177.29

¹HNMR

¹³CNMR

IR1

Mass

MS-NW-7561          
p-tert-butyl-N,N-dimethylaniline
C12H19N             (Mass of molecular ion:    177)

   Source Temperature: 260 °C
   Sample Temperature: 170 °C
   Reservoir, 75 eV

      39.0       1.7
      41.0       2.0
      42.0       1.7
      51.0       1.4
      63.0       1.0
      65.0       1.2
      66.5       3.9
      67.0       1.0
      72.5       1.8
      77.0       3.1
      78.0       1.0
      79.0       1.0
      81.0       1.9
      91.0       3.1
     103.0       1.5
     104.0       1.0
     105.0       1.1
     106.0       1.0
     107.0       1.0
     115.0       1.7
     116.0       1.0
     117.0       1.9
     118.0       2.7
     120.0       3.2
     121.0       3.3
     122.0       2.4
     130.0       1.6
     131.0       1.1
     132.0       1.4
     134.0       4.2
     144.0       1.1
     145.0       1.3
     146.0       7.4
     147.0      12.4
     148.0       2.5
     160.0       4.2
     161.0       3.3
     162.0     100.0
     163.0      12.7
     176.0       1.9
     177.0      27.7
     178.0       3.9

90 MHz in CDCl3

¹H NMR	89.56 MHz
C₁₂ H₁₉ N	0.05 ml : 0.5 ml CDCl₃
p-tert-butyl-N,N-dimethylaniline

    Assign.     Shift(ppm)

      A             7.254
      B             6.703
      C             2.880
      D             1.286

     Hz     ppm     Int.

    654.94   7.313     65
    652.63   7.288     24
    648.25   7.239     29
    645.94   7.213     91
    603.88   6.743     83
    601.56   6.717     25
    597.13   6.668     22
    594.88   6.643     57
    258.00   2.881    685
    115.25   1.287   1000

in CDCl3