2243-56-3

1-萘肼鹽酸鹽(2243-56-3)質譜(MS)

產品名稱:1-萘肼鹽酸鹽

CAS:2243-56-3

分子式:C10H11ClN2

分子量: 194.66

InChI:InChI=1S/C10H10N2.ClH/c11-12-10-7-3-5-8-4-1-2-6-9(8)10;/h1-7,12H,11H2;1H

InChIKey: FYSSYOCJFZSKNW-UHFFFAOYSA-N

Smiles:C12C=CC=CC1=CC=CC=2NN.Cl

Mass

MS-NW-7155          
(1-naphthyl)hydrazine hydrochloride
C10H10N2 HCl        (Mass of molecular ion:    158)

   Source Temperature: 150 °C
   Sample Temperature: 120 °C
   Direct, 75 eV

      16.0       1.1
      17.0       1.5
      18.0       2.5
      28.0       3.8
      35.0       4.7
      36.0      38.1
      37.0       1.6
      38.0      12.7
      39.0       4.1
      50.0       4.7
      51.0       7.3
      52.0       2.1
      57.5       2.9
      58.5       1.8
      61.0       1.7
      62.0       3.8
      63.0       9.2
      63.5       1.2
      64.0       3.5
      64.5       1.2
      65.0       4.1
      65.5       1.4
      66.0       3.0
      70.5       4.0
      71.5       3.9
      74.0       4.7
      75.0       6.3
      76.0       3.6
      77.0       7.5
      78.0       6.0
      79.0       6.5
      86.0       2.1
      87.0       3.3
      88.0       2.8
      89.0       5.4
      90.0       1.2
      98.0       1.4
      99.0       1.2
     100.0       1.0
     101.0       4.2
     102.0       4.6
     103.0       2.6
     113.0       4.8
     114.0       7.8
     115.0      97.4
     116.0      14.1
     117.0       1.5
     126.0       7.9
     127.0      20.6
     128.0      43.5
     129.0       9.0
     130.0       4.5
     131.0       1.2
     140.0       9.7
     141.0      10.9
     142.0      56.8
     143.0      38.6
     144.0       4.5
     155.0       4.0
     156.0       8.5
     157.0       6.4
     158.0     100.0
     159.0      11.9
     177.0       4.7
     179.0       1.7

400 MHz in DMSO-d6

¹H NMR	399.65 MHz
C₁₀ H₁₀ N₂	0.035 g : 0.5 ml DMSO-d₆
(1-naphthyl)hydrazine hydrochloride

    Assign.     Shift(ppm)

      A            10.5
      B             8.9
      C             8.062
      D             7.904
      E             7.54
      F             7.448
      G             7.020

     Hz     ppm     Int.

   4187.37  10.478    112
   3575.41   8.947     38
   3231.61   8.087     38
   3226.66   8.074    312
   3224.65   8.069    197
   3223.73   8.067    191
   3220.07   8.058    295
   3216.77   8.049    334
   3213.66   8.042     67
   3213.11   8.040     72
   3167.50   7.926     69
   3167.13   7.925     69
   3163.65   7.917    356
   3160.35   7.908    349
   3158.52   7.904    247
   3156.33   7.898    243
   3154.13   7.893    400
   3151.38   7.886     66
   3038.18   7.603     37
   3036.90   7.599     37
   3035.98   7.597     38
   3035.44   7.596     37
   3034.89   7.594     39
   3034.52   7.593     40
   3033.97   7.592     39
   3033.24   7.590     43
   3032.69   7.589     45
   3032.14   7.587     48
   3030.31   7.583     56
   3029.76   7.582     55
   3028.47   7.578     69
   3028.11   7.577     69
   3025.73   7.571    167
   3024.45   7.568    151
   3021.51   7.561   1000
   3018.77   7.554    632
   3017.67   7.551    890
   3016.02   7.547    767
   3014.55   7.543    560
   3011.99   7.537    926
   3008.88   7.529    777
   3003.75   7.516     44
   3003.38   7.516     42
   3003.01   7.515     42
   3002.65   7.514     42
   3001.73   7.511     39
   3001.37   7.510     40
   2983.60   7.466    557
   2980.12   7.457     65
   2979.57   7.456     64
   2976.09   7.447    721
   2972.06   7.437     51
   2971.51   7.436     43
   2970.78   7.434     50
   2968.03   7.427    409
   2809.77   7.031    537
   2809.04   7.029    560
   2806.11   7.022     50
   2802.45   7.013    516
   2801.71   7.011    506

in DMSO-d6