19501-58-7

4-甲氧基苯肼鹽酸鹽(19501-58-7)質譜(MS)

產品名稱:4-甲氧基苯肼鹽酸鹽

CAS:19501-58-7

分子式:C7H11ClN2O

分子量: 174.63

InChI:InChI=1S/C7H10N2O.ClH/c1-10-7-4-2-6(9-8)3-5-7;/h2-5,9H,8H2,1H3;1H

InChIKey: FQHCPFMTXFJZJS-UHFFFAOYSA-N

Smiles:C1(NN)=CC=C(OC)C=C1.Cl

¹HNMR

IR1

Raman

Mass

MS-NW-8101          
(p-methoxyphenyl)hydrazine hydrochloride
C7H10N2O HCl        (Mass of molecular ion:    138)

   Source Temperature: 180 °C
   Sample Temperature: 140 °C
   Direct, 75 eV

      15.0       1.5
      17.0       1.9
      18.0       8.4
      26.0       1.1
      27.0       1.6
      28.0       4.2
      29.0       1.9
      35.0       3.1
      36.0      35.7
      37.0       1.3
      38.0      12.3
      39.0       4.9
      40.0       1.0
      41.0       9.2
      42.0       1.2
      50.0       2.8
      51.0       5.1
      52.0       9.0
      53.0       5.5
      54.0       1.4
      55.0       1.2
      62.0       1.6
      63.0       5.7
      64.0       5.3
      65.0       8.6
      66.0       2.8
      67.0       3.5
      68.0       1.3
      69.0       1.3
      77.0       9.5
      78.0       7.6
      79.0       5.1
      80.0      18.7
      81.0       1.8
      90.0       1.6
      91.0       1.2
      92.0       4.3
      93.0       2.3
      94.0       3.1
      95.0      16.7
      96.0       1.4
     106.0       2.3
     107.0       4.8
     108.0       8.0
     122.0      76.1
     123.0      53.9
     124.0       4.1
     136.0       2.5
     137.0       1.8
     138.0     100.0
     139.0       8.7

400 MHz in DMSO-d6

¹H NMR	399.65 MHz
C₇ H₁₀ N₂ O	0.034 g : 0.5 ml DMSO-d₆
(p-methoxyphenyl)hydrazine hydrochloride

    Assign.     Shift(ppm)

      A            10.
      B             7.049
      C             6.880
      D             3.703

     Hz     ppm     Int.

   2822.23   7.062    192
   2820.03   7.057     66
   2815.64   7.046     73
   2813.25   7.040    252
   2809.77   7.031     31
   2757.39   6.900     27
   2753.91   6.891    262
   2751.71   6.886     75
   2747.13   6.874     68
   2744.93   6.869    201
   2741.45   6.860     22
   1480.17   3.704   1000

KBr disc