1833-51-8

二甲基氯甲基苯基硅烷(1833-51-8)紅外圖譜(IR1)

產(chǎn)品名稱:二甲基氯甲基苯基硅烷

CAS:1833-51-8

分子式:C9H13ClSi

分子量: 184.74

InChI:InChI=1S/C9H13ClSi/c1-11(2,8-10)9-6-4-3-5-7-9/h3-7H,8H2,1-2H3

InChIKey: RJCTVFQQNCNBHG-UHFFFAOYSA-N

Smiles:C1([Si](CCl)(C)C)=CC=CC=C1

¹HNMR

¹³CNMR

IR1

Mass

MS-IW-8153          
(chloromethyl)dimethylphenylsilane
C9H13ClSi           (Mass of molecular ion:    184)

   Source Temperature: 230 °C
   Sample Temperature: 150 °C
   Reservoir, 75 eV

      43.0       4.4
      51.0       1.1
      53.0       2.3
      63.0       2.8
      65.0       2.2
      67.5       1.6
      77.0       1.0
      79.0       2.3
      91.0       9.0
      93.0       4.4
      95.0       1.4
     105.0       4.7
     107.0       4.0
     119.0       2.4
     133.0       2.8
     135.0     100.0
     136.0      14.1
     137.0       4.2
     141.0       4.0
     143.0       1.5
     153.0       1.6
     155.0       1.1
     169.0       1.5

400 MHz in CDCl3

¹H NMR	399.65 MHz
C₉ H₁₃ Cl Si	0.05 ml : 0.5 ml CDCl₃
(chloromethyl)dimethylphenylsilane

    Assign.     Shift(ppm)

      A             7.524
      B             7.36
      C             7.35
      D             2.919
      E             0.400

     Hz     ppm     Int.

   3012.45   7.538    134
   3010.62   7.534    156
   3009.40   7.531     56
   3008.06   7.527     80
   3007.32   7.525     71
   3005.49   7.521    111
   3003.91   7.517     82
   3002.93   7.514    180
   2948.24   7.378     43
   2947.14   7.375     48
   2946.66   7.374     54
   2944.82   7.369     52
   2943.73   7.366    152
   2942.75   7.364    204
   2941.65   7.361    209
   2940.55   7.358    136
   2939.09   7.355    107
   2937.13   7.350    101
   2936.40   7.348    106
   2935.55   7.346    127
   2935.06   7.345    127
   2932.74   7.339     36
   2931.64   7.336     32
   2930.30   7.333     50
   1166.63   2.920    547
    163.33   0.409    158
    160.16   0.401   1000
    156.49   0.392    119

in CDCl3