18169-57-8

異丁基三氯硅烷(0309禁空運(yùn))(18169-57-8)質(zhì)譜(MS)

產(chǎn)品名稱(chēng):異丁基三氯硅烷(0309禁空運(yùn))

CAS:18169-57-8

分子式:C4H9Cl3Si

分子量: 191.56

InChI:InChI=1S/C4H9Cl3Si/c1-4(2)3-8(5,6)7/h4H,3H2,1-2H3

InChIKey: GBXOGFTVYQSOID-UHFFFAOYSA-N

Smiles:[Si](Cl)(Cl)(Cl)CC(C)C

¹HNMR

¹³CNMR

IR1

Mass

MS-IW-6980          
trichloroisobutylsilane
C4H9Cl3Si           (Mass of molecular ion:    190)

   Source Temperature: 220 °C
   Sample Temperature: 150 °C
   Reservoir, 75 eV

      27.0       7.5
      28.0       1.0
      29.0       4.3
      38.0       1.0
      39.0      11.1
      40.0       1.7
      41.0      21.4
      42.0       4.1
      43.0      55.0
      44.0       1.9
      49.0       1.0
      53.0       1.2
      55.0       3.7
      56.0       4.4
      57.0       3.9
      63.0       8.8
      65.0       3.4
      98.0       2.4
      99.0       2.5
     100.0       1.8
     101.0       1.8
     112.0       2.3
     113.0       4.5
     114.0       1.8
     115.0       3.0
     117.0       1.1
     125.0       1.3
     133.0      55.8
     134.0       2.9
     135.0      55.8
     136.0       2.9
     137.0      19.7
     138.0       2.1
     139.0      31.9
     140.0       3.7
     141.0      20.6
     142.0       2.0
     143.0       3.9
     153.0       1.4
     154.0       2.8
     155.0       2.4
     156.0       2.0
     157.0       1.1
     174.0       1.1
     175.0     100.0
     176.0       9.6
     177.0      99.7
     178.0       8.7
     179.0      34.3
     180.0       2.8
     181.0       4.4
     189.0       1.9
     191.0       2.0

400 MHz in CDCl3

¹H NMR	399.65 MHz
C₄ H₉ Cl₃ Si	0.05 ml : 0.5 ml CDCl₃
trichloroisobutylsilane

    Assign.     Shift(ppm)

      A             2.108
      B             1.418
      C             1.073

     Hz     ppm     Int.

    856.20   2.143     43
    849.49   2.126     84
    842.77   2.109    106
    836.06   2.092     90
    829.35   2.076     50
    570.19   1.427    487
    563.23   1.410    465
    560.91   1.404     21
    432.50   1.083   1000
    429.81   1.076     60
    425.54   1.065    954
    421.39   1.055     46

in CDCl3