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1719-57-9

氯甲基二甲基氯硅烷(1719-57-9)Raman光譜

產(chǎn)品名稱(chēng):氯甲基二甲基氯硅烷

CAS:1719-57-9

分子式:C3H8Cl2Si

分子量: 143.09

InChI:InChI=1S/C3H8Cl2Si/c1-6(2,5)3-4/h3H2,1-2H3

InChIKey: ITKVLPYNJQOCPW-UHFFFAOYSA-N

Smiles:[Si](Cl)(CCl)(C)C

  • 圖譜
    Mass 

    MS-NW-4934          
chloro(chloromethyl)dimethylsilane
C3H8Cl2Si           (Mass of molecular ion:    142)


       Source Temperature: 260 °C
   Sample Temperature: 180 °C
   Reservoir, 75 eV


          27.0       1.8
      29.0       3.3
      42.0       1.3
      43.0       3.6
      63.0      10.3
      64.0       1.2
      65.0      13.2
      66.0       1.0
      67.0       3.9
      77.0       1.2
      78.0       2.0
      79.0      13.6
      80.0       1.6
      81.0       4.6
      92.0       1.1
      93.0     100.0
      94.0       8.0
      95.0      35.0
      96.0       2.4
      97.0       1.2
      99.0      12.9
     100.0       1.3
     101.0       8.7
     103.0       1.7
     107.0       3.9
     109.0       1.3
     113.0       1.9
     115.0       1.1
     127.0       1.9
     129.0       1.3
     142.0       1.3

parameter in CCl4

90 MHz in CDCl3

  • 圖譜

    1H NMR 300 MHz
    C3 H8 Cl2 Si 10 vol% in CCl4
    chloro(chloromethyl)dimethylsilane
    ChemicalStructure 
        Parameter     ppm  Hz
    
      D(A)         0.550
     
      D(B)         2.892
     
     SCHMIDBAUR,H. & WALDMANN,S. CHEM.BER. 97, 3381 (1964)
     J(A,SI-29):7.3HZ. J(B,SI-29):4.6HZ.
  

         Hz     ppm     Int.


        867.61   2.892    333
    165.00   0.550   1000

  • 圖譜

    1H NMR 89.56 MHz
    C3 H8 Cl2 Si 0.04 ml : 0.5 ml CDCl3
    chloro(chloromethyl)dimethylsilane
    ChemicalStructure 
        Assign.     Shift(ppm)
    
      A             2.948
      B             0.548
     
     J(A,SI-29)=4.3HZ
     J(B,SI-29)=7.2HZ
  

         Hz     ppm     Int.


        264.13   2.950    329
     52.75   0.589     36
     49.13   0.549   1000
     45.56   0.509     39

in CDCl3

  • 圖譜

liquid film

  • 圖譜

  • 圖譜

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