16646-44-9

四烯丙氧基乙烷(16646-44-9)核磁圖(¹HNMR)

產(chǎn)品名稱:四烯丙氧基乙烷

CAS:16646-44-9

分子式:C14H22O4

分子量: 254.32

InChI:InChI=1S/C14H22O4/c1-5-9-15-13(16-10-6-2)14(17-11-7-3)18-12-8-4/h5-8,13-14H,1-4,9-12H2

InChIKey: BXAAQNFGSQKPDZ-UHFFFAOYSA-N

Smiles:C(OCC=C)(OCC=C)C(OCC=C)OCC=C

Mass

MS-NW-5246          
1,1,2,2-tetrakis(allyloxy)ethane
C14H22O4            (Mass of molecular ion:    254)

   Source Temperature: 260 °C
   Sample Temperature: 190 °C
   Reservoir, 75 eV

      27.0       2.4
      28.0       2.7
      29.0       2.5
      31.0       2.2
      39.0      10.9
      40.0       1.6
      41.0     100.0
      42.0       4.5
      43.0       3.7
      54.0       1.0
      55.0       5.6
      57.0       6.5
      67.0       1.6
      69.0       1.4
      71.0       2.5
      79.0       2.4
      81.0      49.1
      82.0       3.5
      87.0       1.0
      99.0       2.5
     127.0      26.9
     128.0       2.3
     140.0       1.9
     185.0       2.5

90 MHz in CDCl3

¹H NMR	89.56 MHz
C₁₄ H₂₂ O₄	0.04 ml : 0.5 ml CDCl₃
1,1,2,2-tetrakis(allyloxy)ethane

    Assign.     Shift(ppm)

      A             5.91
      B             5.30
      C             5.18
      D             4.505
      E             4.17

     Hz     ppm     Int.

    551.63   6.160     74
    546.06   6.098    144
    541.50   6.047    109
    540.69   6.038     97
    536.00   5.985    185
    534.38   5.967    141
    530.69   5.926    122
    528.81   5.905    248
    526.25   5.876     35
    524.25   5.854    194
    523.44   5.845    171
    521.94   5.828     30
    521.19   5.820     37
    520.44   5.812     49
    518.75   5.793    316
    516.31   5.765     40
    515.31   5.754     39
    513.50   5.734    201
    484.56   5.411    161
    483.06   5.394    338
    482.38   5.387    320
    480.94   5.371    488
    479.50   5.354    247
    477.38   5.331     37
    477.06   5.327     34
    473.19   5.284     45
    472.75   5.279     49
    472.19   5.273     40
    470.00   5.248    241
    468.69   5.234    437
    467.44   5.220    376
    466.63   5.211    353
    465.75   5.201    331
    464.38   5.186    256
    463.75   5.179    272
    462.25   5.162    158
    460.06   5.137    206
    458.69   5.122    298
    457.88   5.113    194
    457.38   5.107    208
    456.63   5.099    256
    455.38   5.085    135
    403.50   4.506   1000
    387.06   4.322     30
    381.56   4.261     33
    380.31   4.247     43
    379.69   4.240     55
    378.44   4.226    101
    376.81   4.208    458
    375.56   4.194    785
    374.19   4.179    490
    372.88   4.164    159
    371.75   4.151    373
    371.13   4.144    397
    370.31   4.135    597
    369.94   4.131    593
    368.88   4.119    365
    363.31   4.057     36
    363.00   4.054     35
    361.75   4.040     30

in CDCl3