1HNMR)的核磁圖,紅外圖譜,Raman光譜,質(zhì)譜等圖譜" /> 1HNMR)" />

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返回ChemicalBook首頁(yè)>CAS數(shù)據(jù)庫(kù)列表>13548-69-1更多圖譜> 2,7-二氨基芴二鹽酸鹽(13548-69-1)核磁圖(1HNMR)

13548-69-1

2,7-二氨基芴二鹽酸鹽(13548-69-1)核磁圖(1HNMR)

產(chǎn)品名稱:2,7-二氨基芴二鹽酸鹽

CAS:13548-69-1

分子式:C13H14Cl2N2

分子量: 269.17

InChI:InChI=1S/C13H12N2.2ClH/c14-10-1-3-12-8(6-10)5-9-7-11(15)2-4-13(9)12;;/h1-4,6-7H,5,14-15H2;2*1H

InChIKey: QJXYCUYLZDQRIN-UHFFFAOYSA-N

Smiles:C12C=CC(N)=CC=1CC1=CC(N)=CC=C21.Cl.Cl

  • 圖譜
    Mass 

    MS-NW-2332          
2,7-fluorenediamine dihydrochloride
C13H12N2 2HCl       (Mass of molecular ion:    196)


       Source Temperature: 200 °C
   Sample Temperature: 140 °C
   Direct, 75 eV


          18.0       2.7
      28.0       1.0
      35.0       2.4
      36.0      22.5
      38.0       7.4
      63.0       1.0
      70.5       1.0
      83.5       6.0
      84.0       1.9
      97.5       7.0
      98.0       8.5
      98.5       1.1
     115.0       1.0
     139.0       2.3
     140.0       1.4
     141.0       1.0
     151.0       2.4
     152.0       2.6
     153.0       1.0
     166.0       1.3
     167.0       5.9
     168.0       4.4
     178.0       2.2
     179.0       2.5
     180.0      11.7
     181.0       2.1
     193.0       1.1
     194.0       1.3
     195.0      35.7
     196.0     100.0
     197.0      14.8
     198.0       1.1

400 MHz in D2O

  • 圖譜

    1H NMR 399.65 MHz
    C13 H12 N2 0.042 g : 0.5 ml D2O
    2,7-fluorenediamine dihydrochloride
    ChemicalStructure 
        Assign.     Shift(ppm)
    
      A             7.339
      B             7.294
      C             7.263
      D             3.134
     
     SOLVENT SIGNAL REMOVED
  

         Hz     ppm     Int.


       2933.72   7.341    674
   2932.62   7.338    704
   2926.88   7.324     26
   2920.90   7.309    351
   2912.96   7.289   1000
   2905.88   7.272    631
   2903.93   7.267    559
   2897.71   7.251    224
   2895.75   7.246    211
   1252.44   3.134    589

KBr disc

  • 圖譜

nujol mull

  • 圖譜

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