13CNMR)的核磁圖,紅外圖譜,Raman光譜,質(zhì)譜等圖譜" /> 13CNMR)" />

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109-01-3

N-甲基哌嗪(109-01-3)核磁圖(13CNMR)

產(chǎn)品名稱:N-甲基哌嗪

CAS:109-01-3

分子式:C5H12N2

分子量: 100.16

InChI:InChI=1S/C5H12N2/c1-7-4-2-6-3-5-7/h6H,2-5H2,1H3

InChIKey: PVOAHINGSUIXLS-UHFFFAOYSA-N

Smiles:N1(C)CCNCC1

  • 圖譜
    Mass 

    MS-NW-1596          
1-methylpiperazine
C5H12N2             (Mass of molecular ion:    100)


       Source Temperature: 240 °C
   Sample Temperature: 180 °C
   Reservoir, 75 eV


          15.0       5.5
      18.0       1.9
      26.0       1.1
      27.0       3.9
      28.0      12.1
      29.0      10.3
      30.0       9.1
      41.0       3.7
      42.0      24.5
      43.0      35.2
      44.0      13.2
      45.0       1.4
      54.0       1.7
      55.0       1.5
      56.0      14.9
      57.0       9.6
      58.0     100.0
      59.0       3.5
      70.0       3.9
      71.0       2.2
     100.0      39.1
     101.0       2.4

90 MHz in CDCl3

  • 圖譜

    1H NMR 89.56 MHz
    C5 H12 N2 0.04 ml : 0.5 ml CDCl3
    1-methylpiperazine
    ChemicalStructure 
        Assign.     Shift(ppm)
    
      A             2.884
      B             2.369
      C             2.264
      D             1.72
  

         Hz     ppm     Int.


        264.13   2.950    109
    259.81   2.901    129
    254.63   2.844    213
    216.50   2.418    165
    213.38   2.383     74
    211.31   2.360    138
    206.75   2.309     97
    202.81   2.265   1000
    200.06   2.234     28
    154.13   1.721    123

in CDCl3

  • 圖譜

CCl4 solution

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liquid film

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