N-甲基對硝基苯胺(100-15-2)核磁圖(1HNMR)
InChI:InChI=1S/C7H8N2O2/c1-8-6-2-4-7(5-3-6)9(10)11/h2-5,8H,1H3
InChIKey: XIFJZJPMHNUGRA-UHFFFAOYSA-N
Smiles:C1(NC)=CC=C([N+]([O-])=O)C=C1
-
Mass
MS2015-05133CW
N-methyl-p-nitroaniline
C7H8N2O2 (Mass of molecular ion: 152)
Source Temperature: 250 °C
Sample Temperature: 20 °C
Direct, 70 eV
15.0 2.9
18.0 1.7
26.0 1.2
27.0 3.2
28.0 9.7
30.0 7.8
37.0 2.3
38.0 5.6
39.0 10.7
40.0 1.6
41.0 3.0
42.0 2.8
46.0 2.7
50.0 15.0
51.0 12.3
52.0 8.2
53.0 4.9
54.0 3.3
55.0 2.6
61.0 1.8
62.0 4.4
63.0 13.0
64.0 10.4
65.0 30.3
66.0 4.9
67.0 2.9
68.0 1.5
73.0 1.0
74.0 6.4
75.0 5.0
76.0 10.2
77.0 43.2
78.0 15.4
79.0 29.3
80.0 4.1
90.0 3.9
91.0 7.3
92.0 1.6
93.0 1.5
94.0 16.0
95.0 1.1
104.0 10.1
105.0 17.8
106.0 27.8
107.0 2.5
120.0 1.5
122.0 57.6
123.0 4.7
136.0 5.3
150.0 1.9
151.0 3.7
152.0 100.0
153.0 10.2
400 MHz in DMSO-d6
90 MHz in CDCl3
in CDCl3
-
| 1H NMR |
399.65 MHz |
| C7 H8 N2 O2
|
0.033 g : 0.5 ml DMSO-d6
|
| N-methyl-p-nitroaniline
|
 |
Assign. Shift(ppm)
A 8.022
B 7.32
C 6.615
D 2.811
90MHZ:HSP-03-231 IN CDCL3
|
Hz ppm Int.
3210.69 8.034 329
3208.74 8.029 119
3203.37 8.016 127
3201.42 8.011 339
2928.71 7.329 63
2923.95 7.317 62
2653.32 6.640 35
2648.56 6.628 347
2646.48 6.622 124
2644.04 6.616 54
2641.24 6.609 125
2639.16 6.604 337
1126.10 2.818 1000
1120.97 2.805 997
-
| 1H NMR |
89.56 MHz |
| C7 H8 N2 O2
|
0.034 g : 0.5 ml CDCl3
|
| N-methyl-p-nitroaniline
|
|
Assign. Shift(ppm)
A 8.087
B 6.529
C 4.7
D 2.938
|
Hz ppm Int.
732.31 8.177 22
729.13 8.142 233
727.00 8.118 64
721.94 8.061 68
719.81 8.038 257
716.63 8.002 27
589.25 6.580 224
587.06 6.555 61
582.06 6.500 51
579.94 6.476 195
263.13 2.939 1000
-
