2,2'-METHYLIMINOBIS(ACETALDEHYDE DIETHYL ACETAL)(6948-86-3) IR1
Product Name2,2'-METHYLIMINOBIS(ACETALDEHYDE DIETHYL ACETAL)
CAS6948-86-3
Molecular FormulaC13H29NO4
Molecular Weight263.37
InChIInChI=1S/C13H29NO4/c1-6-15-12(16-7-2)10-14(5)11-13(17-8-3)18-9-4/h12-13H,6-11H2,1-5H3
InChIKey DPLOXPRJCFWURN-UHFFFAOYSA-N
SmilesC(OCC)(OCC)CN(C)CC(OCC)OCC
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MassMS-NW-5835 N,N-bis(2,2-diethoxyethyl)methylamine C13H29NO4 (Mass of molecular ion: 263)
Source Temperature: 260 °C Sample Temperature: 190 °C Reservoir, 75 eV
15.0 3.4 18.0 1.8 19.0 1.7 26.0 1.7 27.0 6.6 28.0 3.8 29.0 15.2 30.0 1.3 31.0 14.4 41.0 1.9 42.0 11.2 43.0 6.8 44.0 11.9 45.0 10.5 46.0 1.7 47.0 33.1 55.0 1.2 56.0 1.4 57.0 4.7 58.0 14.9 59.0 27.1 60.0 1.5 61.0 10.1 70.0 3.1 71.0 2.3 72.0 11.0 73.0 4.0 74.0 1.0 75.0 25.5 76.0 1.0 82.0 1.5 84.0 2.9 85.0 1.6 86.0 4.9 88.0 1.1 89.0 5.0 96.0 1.6 97.0 1.2 98.0 2.1 99.0 1.1 100.0 3.9 101.0 4.1 102.0 6.5 103.0 30.9 104.0 1.8 114.0 31.7 115.0 2.9 116.0 28.5 117.0 2.8 125.0 1.2 129.0 2.6 130.0 2.1 132.0 2.6 142.0 1.1 146.0 13.8 147.0 3.7 158.0 2.6 160.0 100.0 161.0 8.7 171.0 1.6 172.0 16.0 173.0 2.3 174.0 1.1 204.0 3.0 217.0 4.3 218.0 13.0 219.0 3.1
90 MHz in CDCl3
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1H NMR 89.56 MHz C13 H29 N O4 0.04 ml : 0.5 ml CDCl3 N,N-bis(2,2-diethoxyethyl)methylamine 
Assign. Shift(ppm)
A 4.608 B *1 3.659 C *1 3.526 D 2.652 E 2.408 F 1.212 J(A,D)=5.2HZ. J(B,F)=J(C,F)=7.0HZ. J(B,C)=9.3HZ.
Hz ppm Int.418.38 4.672 56 413.13 4.613 133 407.88 4.555 75 339.19 3.788 48 337.06 3.764 59 332.06 3.708 60 331.13 3.698 68 329.88 3.684 181 324.06 3.619 180 322.75 3.604 199 317.13 3.541 179 315.69 3.525 84 314.75 3.515 56 310.19 3.464 67 307.75 3.437 49 240.13 2.682 208 234.88 2.623 196 215.63 2.408 321 115.38 1.289 450 108.31 1.210 1000 101.25 1.131 386
in CDCl3
liquid film
