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Back ChemicalBook Home>CAS DataBase List>37577-28-9More Spectrum> D-(+)-Norephedrine(37577-28-9) 13C NMR

37577-28-9

D-(+)-Norephedrine(37577-28-9) 13C NMR

Molecular FormulaC9H13NO

Molecular Weight151.21

  • D-(+)-Norephedrine(37577-28-9) <sup>13</sup>C NMR
    Mass

    MS-IW-9093          
    (1S,2R)-(+)-2-amino-1-phenyl-1-propanol
    C9H13NO             (Mass of molecular ion:    151)
    

       Source Temperature: 210 °C
       Sample Temperature: 150 °C
       Reservoir, 75 eV
    

          18.0       5.9
          27.0       1.5
          28.0       2.5
          39.0       2.5
          41.0       1.1
          42.0      12.7
          43.0       1.8
          44.0     100.0
          45.0       3.0
          50.0       1.7
          51.0       4.4
          52.0       1.3
          56.0       1.1
          63.0       1.5
          65.0       2.6
          70.0       1.6
          71.0       2.1
          77.0       8.7
          78.0       2.0
          79.0       4.4
          89.0       1.6
          90.0       1.2
          91.0      12.6
          92.0      13.6
          93.0       1.1
         104.0       1.2
         105.0       5.5
         106.0       3.5
         107.0       2.1
         115.0       2.2
         116.0       1.6
         117.0       4.0
         118.0       2.6
         132.0       8.0
         133.0       8.2
         134.0       1.3
    

400 MHz in CDCl3

  • D-(+)-Norephedrine(37577-28-9) <sup>13</sup>C NMR

    1H NMR 399.65 MHz
    C9 H13 N O 0.041 g : 0.5 ml CDCl3
    (1S,2R)-(+)-2-amino-1-phenyl-1-propanol
    ChemicalStructure
        Assign.     Shift(ppm)
    A 7.31 B 7.26 C 4.429 D 3.057 E 2.3 F 0.925

         Hz     ppm     Int.
    

       2930.54   7.333     70
       2929.32   7.330    105
       2927.73   7.326     45
       2923.34   7.315    191
       2922.12   7.312    282
       2920.90   7.309    224
       2917.48   7.301    115
       2915.16   7.295    416
       2909.67   7.281    293
       2907.96   7.277    547
       2905.40   7.270    153
       2903.93   7.267    197
       2902.95   7.264    225
       2901.37   7.260    267
       2898.44   7.253    104
       2895.75   7.246    200
       2892.70   7.239     45
       2890.87   7.234     42
       2888.92   7.229     64
       2887.21   7.225     33
       1772.46   4.436    246
       1767.58   4.423    255
       1234.01   3.088     37
       1229.00   3.076     50
       1227.42   3.072    127
       1222.53   3.060    133
       1220.95   3.056    137
       1216.06   3.043    129
       1214.60   3.040     53
       1209.59   3.027     39
        930.05   2.328     34
        372.92   0.934    982
        366.33   0.917   1000
    

in CDCl3

  • D-(+)-Norephedrine(37577-28-9) <sup>13</sup>C NMR

KBr disc

  • D-(+)-Norephedrine(37577-28-9) <sup>13</sup>C NMR

nujol mull

  • D-(+)-Norephedrine(37577-28-9) <sup>13</sup>C NMR

  • D-(+)-Norephedrine(37577-28-9) <sup>13</sup>C NMR

D-(+)-Norephedrine(37577-28-9) 13C NMR Atlas of Related Products

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